The molecules don't separate because of their size. He said big molecules, little molecules. They separate because of the various effects the solvent system and the solid phase has on the mobile phase, where the mobile phase is the mixture you are trying to separate. The solid phase is the sand. You want to choose a solvent system that will allow a greater distance between the THC and CBD phase as it runs through the column. It has to do with polarity and a few other factors. What he is doing is called flash chromatography, which is column chromatography with the use of air pressure to force the mobile phase through the solid phase. Also, depending on the solvent system, it is possible for the order of the molecules to change--he said CBD will come off first, but that wouldn't be guaranteed as it depends on the solvent system. I am not familiar with weed chemistry, so I cannot contribute any solvent systems that would be helpful, but I am sure those are readily described.
It is easy . You need pure Silicon Dioxide (sand) A glass tube to hold the material and filter . The liquid would be the oil mixed with some ethanol Apply pressure or suction from below and that's it
Why is the thc absorbed oppose to the CBD? Would this process work with oil with a higher percentage of THC as in not extracted from hemp but high CBD cannabis?
using the glass column and dye was smart of you. helps us a lot to get the picture of what is happening during the separation process going on inside the metal vessels.
The whole coffee machine bit is pretty easily achieved *I believe evergreen bark is loaded with CBD. Polarity *pentane is oftentimes used (you ever see big crystals formulate it's likely bonded to pentane to create what people call diamonds / diamond mining) Coffee maker bit Just steam distill easy as pie can run a pump easily too. Can have a rotating changer tray like a 6 disc changer for separation by density. All too easy
You honestly make this sound so much easier than I imagine it really is. Very easy to comprehend! You also seem like a really cool dude that I'd share a J with. Keep it up man, it's inspiring.
@@typhoonfire8 well, i dont think ppl care. They just dont feel like paying $100 for a few grams when they could make 50% pure on their own for $10 lol
what is the glass chromatography system you showed us? Do I just buy the chromatography glass column and a gas tank? I have no idea what I am meant to be buying, as it is obviously all in separate parts. Your channel is amazing!
If I'm only getting THC out, does it take longer the same amount of time? And do you do it over and over a few times by rerunning the same fluid or keep adding extra fluid for each run thru the sand? What kind of sand would you suggest? Last thing, what kind of fluid exactly? (Sorry for all the questions at once. Lol.)
I'm really interested in making high quality CBD oils and getting it to the hands of people who really need it. I've extracted THC using half Butane half Everclear. I felt like i did a pretty good job but it was it was for my own consumption. I really wanna study and help people in need. Your videos are a really big help. Is there any major things that i should keep and eye out for when extracting CBD and turning it into pure CBD. Thanks again for the upload of the awesome videos.
Have you tried with a single cup coffee maker? Take it apart, reroute the water lines and add your chromatography tube along side of the machine with an additonal water line routed from the bottom of the tube into the drip spout. Utilize the water pump as a pressure pump. Pressure may be an issue, or pump timing. Find the pressure or low water switch and cut it away from the pump and add a switch to it so it doesnt stop automatically to hopefully keep the oressure for the tube. Love the idea of building a consumer Oil maker!!! Dont even think it would be that difficult. Just a thought 🤷♂️😊 awesome videos. Love the ingenuity!
Could you use an espresso machine? Very small scale fill the basket with the sand or make a column shaped basket. Then put the product on top of the sand and switch on they create 15-21bar of pressure so don't see why it wouldn't work 🤷🏻♂️ worth a try.
In your written explanation, there is a incorrect word, "Absorbent", should be "Adsorbent". Similar, but not at all the same. You have the best column purification video, that I have seen. Good Job and thank you presenting the info.
Some cheap chemistry equipment , some silicon caulking , gaskets and a cheap walmart vacuum and you will be in business with a capital B in this regard. Not to mention all your friends will be jealous that you can make for 15 bucks what costs them 130 bucks with a GOOD sale going on
We try to use easily understandably terminology so everyone can understand what we are doing, however silica gel is a granular, vitreous, porous form of silicon dioxide and in many parts of the world, silica is the major constituent of sand, but thanks for the constructive criticism, we will take better care of explaining ourselves in the future :)
Thank you very much for showing this I am very interested in this process could you do more videos on this in the bigger equipment. Also besides the colloum what other pieces of equipment are needed for smaller experiments. Again thank you
yo do would you know the ways of making this a basic but still like $100 -$500 set up not even like somthing a one man set up could make some personal CBD from hemp
🤔 Any links to your R&D department? There's a cure to the task 😊 But when you say "coffee maker" it opens a pallet of cans of worms 😁 but it is doable.
What if you place sand in the filter of the coffee machine, place gas tube and seal the coffee machine so the pressure can be kept within as much as possible. If the coffee can be assigned for CBD making than you can drill hole for the gas tube to minimize the gas escaping and create the pressure needed. Just was thinking, I am applied chemistry student and I am very interested in the topic of CBD extractions.
We put our extraction machinery online here in New Mexico. 50,000 lbs of input material every day. Roughly 2500 kilos of winterized crude production daily. 💪 Distillate to the same capacity by March, 2020.
I can not work out what "liquid" you used in the filtration system, was it ethonal. Iv looked through the comments and you have soaked up all the compliments but havent answered any questions so if anyone knows what liquid he used that would be appreciated
Fill water tank of cheap coffee machine with sand, disconnect the heating circuit of the water pre-filter, would the pump then create pressure, evaporate off as usual etc? Great videos man.
Have you guys tried liquid extraction if you did with what solvent? Also curious about what sand is used. Reason for askin, very few people have access to GC equipment to ensure how much thc goes through. Thanx for the video.
i generally use solvent dispersion in a piece of pre washed hemp paper, that's called paper chromatography, and it's based in the different speed of propagation of different compounds trough convection in a solid, you will drop the solution and check the side that countains thc, i don't remember wich side it's, one side will have thc and the other cbd, cut the cbd side, wash the cbd paper with isopropyl alcohol and repeat the process as much as you like, you can buy a fluorsilicon pot in the cooking items in any supermarket, fluorsilicon is shatter proof, to collect the hash in one ball you might want to freeze that.
fss1704 hey I’m looking into making my own CBD crystals and the way you’re explaining it makes sense but would it be possible for you to maybe make a video on the presses and steps you take when doing paper chromatography I think that would help a lot of people like myself who just want to make this at home thank you.
I don’t have access to nmr at the moment, and my TLCs are a mess. Wondering what solvent system you’re using and what the r.f. of CBD and THC is for you? I’m running 10% EtOAc/Hexane, but I’m getting some streaking spots.
LOVE the fact ur trying to share this info. In all honesty thou I reakon I've got more chance of sprouting a fanny than than SUCCESSFULLY doing this in the kitchen😂😂
It's definitely not the easiest project to take on, however people had been asking us for a long time how it worked so we thought it was high time we at least tried to explain
You say that for purity you need to pass it through the column multiple times, does that mean you put new sand in the column each time? Otherwise you are passing your clean(er) material through the contamination again or am I missing something?
Great video i love knowledge, maybe this will help a coffee maker the filter chamber isn't sealed, what about using a espresso machine, I'm not sure but I think it has a pressurized chamber. You might consider using something like that.
My concern is about the solvant that is used. Is ethanol the solvant used for the industrial / advanced material version ? I thought your company used critical-CO2 for the cbd extraction, as a carrier/solvant ? Is it for the cristals or the oil ?
Hi Celine, nope we only extract using a C02 extraction method. Our previous video just gives people the power to make their own oil at home, if they can't afford to buy it
could you make the process automated , using pumps to recirculate the product x number of times need valves and switches but should be able to be done with relay logic no cpu needed just asking i have no clue on viscisity etc
hi endoca, big fan, loyal customer. still a bit confused how to use my crystals. just ran out of 50mg raw cbd caps and raw oil 150mg so will experiment as i purchased crystals in bulk but never figured out a comparable dose- any advice? my current pain mgmt for crippling rheumatoid arthritis is 10mg raw cbd cap in am, 150mg raw oil-4-6 drops- midday, 50mg raw cbd cap at night and hemp cream hands and elbows... endoca helped me reduce my rx.oxycodone 75% in about 4 weeks... thank you for that. =^..^=
Hi there Kimi! Thank you for your kind words. If you're interested in experimenting, it really depends on how strong of an oil you want. If you want something close to our formula - it's quite simple: 500mg in 10ml of oil will yield a 5% oil, 1500mg in oil will yield 15% and so forth. Otherwise, if you like that sort of thing, you can vape the crystals. Here, the dosing is a bit more subjective and it is more up to you how much you add to your vape at one time. If you have any more questions, come on down to our website and feel free to chat with our dedicated care team, who will surely be able to provide you with a lot more information. :)
You need a tube, some sand, and some liquid? What tube? What kind of sand? What kind of liquid? This video is so damn vague you really didn't tell anything about the process at all, wow! When people make videos like this, it's not to share information but to sell information. Thanks for nothing.
Hey Jessica, you will need chromatography equipment, this is not a video for people to do at home with utensils found around the house. We tried to find a way to do this, but it proved impossible, so we shared with you the basics of how we make our pure CBD, however you will need the appropriate equipment to make it yourself
i generally use solvent dispersion in a piece of pre washed hemp paper, that's called paper chromatography, and it's based in the different speed of propagation of different compounds trough convection in a solid, you will drop the solution and check the side that countains thc, i don't remember wich side it's, one side will have thc and the other cbd, cut the cbd side, wash the cbd paper with isopropyl alcohol and repeat the process as much as you like, you can buy a fluorsilicon pot in the cooking items in any supermarket, fluorsilicon is shatter proof, to collect the hash in one ball you might want to freeze that.
I dont understand a couple things. how do you know when the filtering of cbd is done and the thc starts? does the thc afterwards just get stuck in there and never come out? I would be scared of getting some thc in the cbd. Can you help me understand this?
Hi I am suffering from depression almost all my life live in England I don't think we can make in house I think it is against the law we have to buy from the shop
It's always better to buy from a reputable source as that way you know exactly what you are getting. Making it at home can be very difficult and the results unpredictable
That's exactly what I thought! I was looking for this comment. I imagine it would work. What I would do, theoretically, is disable to heating unit (and any alarms the system might have for it like an auto off), putting pure sand in the area for the "puck" of finely ground coffee, then have the machine push it through. Just use a small enough amount to test it and pray it works
Endoca CBD thanks for the reply, I forgot to specify in my query whether this method results in crystals which contain only the Cannabidiol phytocannabinoid, as i understand there are many cannabinoids in flower?
My thoughts would be if you vaporize the materials at a certain temp, then they liquefy at a lower temp. Now if you you do this temp on the solution at start, then it would liquefy unwanted matter. I believe your hypothesis on the pressure is necessary. My question is you used water as your solvent and slowly added pressure, this eventually would generate heat, as you warm to a certain temp all of the carbon and non crystalline objects would be forced to the bottom. If you are having problems understanding where I am going at this point, research the cubic zarconia creation methods. You have to understand you are working with a crystalline.
+Rodrigo Delgado take the paper filter and do paper chromatography. No fking equipment nor special solvent needed, just a piece of paper and isopropyl alcohol.
Let me say this, thank God for cannabidiol because it is my medicine as without it my world is too stressful, I feel centered when I use it, 1 dose keeps me going for a week.
What liquid was in the round bottom flask... if trying to make crystals you could use a ratio of sugar maybe 3:1.... 3 parts marijuana and 1 part sugar water then dehydrate with coffee machine... maybe the THC would crystallize out with sugar..
#Endoca CBD You got something really good going with this bud. Keep doin' what you're doin' 'cuz the information you give is greatly appreciated. Would be nice if you had a list and/or instructions...along with where can a simple man like myself find something like this for the future? Homemade etc...
No, crystals are decarboxylated as they are CBD. We can not give medical advice, even for pets, best to work out what dose your dog needs, it is related to weight and size. Hope that helps!
You say that first comes out the cbd. Does the thc eventually comes out or the sand doesn't alloud thc to pass trough. If the thc passes trough when woukd I know its time to get out the destilated liquid to be sure that I only have CBD? Thank you
We use CBD extracts, from our CBD rich hemp plants, therefore we don't actually have THC, or have only very minute amounts which are within the legal limits, in our plant material and therefore our extracts before we get to this point
paper chromatography, i used it a lot to separe the substances in a big page of phun subs, to separe the real substance in the middle of the garbage, i removed the "LCD" from the paper and returned that crap to the seller to sell the unknown shit that was mixed.
This depends on the strength of your CBD oil as every extract will have varying quantities of CBD inside, so there is no black and white answer to this unfortunately, too many variables involved
Giving weed has an "average" 12% cannabinoid content and assuming you're extracting an indica with 80%CBD by volume, some 8,18% of the mass of the cannabis will be cbd, so if you could theoretically magically without any loss extract 100% of the cbd of the plant to crystals you'd need some 13KG of cannabis per kg of crystal.
could you let me know what solvent you are putting with the exstract also what is the gas you had in the tank any advese as im tring it to treet my medcal problems thanks for the vid
Please more details which kind of solvent are you using? is there a way do do a good extract at home? so on and so forth i bet here are some more patients that could need this information.
Hey max, we have another video on our channel showing you how to extract your own oil at home here ua-cam.com/video/fYMCA_Tg_vk/v-deo.html this is a video to extract crystals from the CBD extract
For at-home solvents, we usually recommend using ethanol - the more pure the better, but make sure that it is not a kind of alcohol that is toxic for consumption. After all, the oils and crystals are often ingested. :)
The molecules don't separate because of their size. He said big molecules, little molecules. They separate because of the various effects the solvent system and the solid phase has on the mobile phase, where the mobile phase is the mixture you are trying to separate. The solid phase is the sand. You want to choose a solvent system that will allow a greater distance between the THC and CBD phase as it runs through the column. It has to do with polarity and a few other factors. What he is doing is called flash chromatography, which is column chromatography with the use of air pressure to force the mobile phase through the solid phase. Also, depending on the solvent system, it is possible for the order of the molecules to change--he said CBD will come off first, but that wouldn't be guaranteed as it depends on the solvent system. I am not familiar with weed chemistry, so I cannot contribute any solvent systems that would be helpful, but I am sure those are readily described.
i need a discription like this for what happens in a honeybee extractor +lightergas (grinded buds)
@@zap7026 what is a honeybee extractor?
It is easy .
You need pure Silicon Dioxide (sand)
A glass tube to hold the material and filter .
The liquid would be the oil mixed with some ethanol
Apply pressure or suction from below and that's it
you dont use ethanol for this process
Have you done it?
Easy? For you who must be a real scientist!
Catherine S. Todd not really, just takes some cash for a CRC and a closed loop and a lil bit of understanding on how crystals are formed
Why is the thc absorbed oppose to the CBD? Would this process work with oil with a higher percentage of THC as in not extracted from hemp but high CBD cannabis?
What happens to the other Cannabinoids?? Their are over a 100 cannabinoids? SO I am curious how do you know that Pure CBD is left crystalized? Thanks
you work for gustavo fring or what?!?
What is the mixture you use for eluent? Are you doing gradients 50/50 or single solvent? Also have you thought about dry column vacuum chromatography?
oh man, you look so happy as if you had some of those crystals already 🤣 nicely done
Henry is always happy! :)
using the glass column and dye was smart of you. helps us a lot to get the picture of what is happening during the separation process going on inside the metal vessels.
Glad you enjoy our content!
Sweeeeet! That week I spent at college is finally going to pay off 🤓🤑
Congratulations!
Watch that and tell me if it's really that easy to remove every single thing but CBD. I wouldn't touch your product
@@PesoTheDaddy Much easier if he started with 20% CBD 0.5%THC plant resin oil
I never saw any one like you who give so much ans of comments I think you are great learner and curious person
Very cool. Is there a specific size of sand granules? specific type of sand ?
He is killin me with the coffee machine bit. Great vids sweetie very informative
The whole coffee machine bit is pretty easily achieved *I believe evergreen bark is loaded with CBD. Polarity *pentane is oftentimes used (you ever see big crystals formulate it's likely bonded to pentane to create what people call diamonds / diamond mining)
Coffee maker bit
Just steam distill easy as pie can run a pump easily too.
Can have a rotating changer tray like a 6 disc changer for separation by density.
All too easy
You honestly make this sound so much easier than I imagine it really is. Very easy to comprehend! You also seem like a really cool dude that I'd share a J with. Keep it up man, it's inspiring.
@@typhoonfire8 well, i dont think ppl care. They just dont feel like paying $100 for a few grams when they could make 50% pure on their own for $10 lol
@@TurboHommy well I agree with the comment above. This video is going to hurt people. And there's nothing funny about that
what is the glass chromatography system you showed us? Do I just buy the chromatography glass column and a gas tank? I have no idea what I am meant to be buying, as it is obviously all in separate parts.
Your channel is amazing!
If I'm only getting THC out, does it take longer the same amount of time? And do you do it over and over a few times by rerunning the same fluid or keep adding extra fluid for each run thru the sand? What kind of sand would you suggest? Last thing, what kind of fluid exactly? (Sorry for all the questions at once. Lol.)
Henry, where is the link to the next video? Is it available yet? BTW - thank you for your excellent educational series.
I'm really interested in making high quality CBD oils and getting it to the hands of people who really need it. I've extracted THC using half Butane half Everclear. I felt like i did a pretty good job but it was it was for my own consumption. I really wanna study and help people in need. Your videos are a really big help. Is there any major things that i should keep and eye out for when extracting CBD and turning it into pure CBD. Thanks again for the upload of the awesome videos.
Thank you for sharing your knowledge, love, and passion for the cannabis culture and the community. Respect to you brother. 🙏🌱☘🍀🍁
Your welcome! Thanks for watching 😁
Have you tried with a single cup coffee maker? Take it apart, reroute the water lines and add your chromatography tube along side of the machine with an additonal water line routed from the bottom of the tube into the drip spout. Utilize the water pump as a pressure pump. Pressure may be an issue, or pump timing. Find the pressure or low water switch and cut it away from the pump and add a switch to it so it doesnt stop automatically to hopefully keep the oressure for the tube. Love the idea of building a consumer Oil maker!!! Dont even think it would be that difficult. Just a thought 🤷♂️😊 awesome videos. Love the ingenuity!
Are you part of a manufacturing company that sells these products “Endoca?” Guess I will research the name. Thanks for the videos! Knowledge is power.
Yep, Henry is the CEO of Endoca :) Exactly, knowledge is power!
Could you use an espresso machine? Very small scale fill the basket with the sand or make a column shaped basket. Then put the product on top of the sand and switch on they create 15-21bar of pressure so don't see why it wouldn't work 🤷🏻♂️ worth a try.
Is there any hands on classes that you guys do anywhere, I'm super interested in making this a better world to live in.
Get medical marijuana for recreational use available everywhere every state and this will be a better place
I love this channel and this man is what people should think of when they hear “stoner” not all of us are dumbfucks
In your written explanation, there is a incorrect word, "Absorbent", should be "Adsorbent". Similar, but not at all the same. You have the best column purification video, that I have seen. Good Job and thank you presenting the info.
Thanks!
If you can't apply pressure above then apply negative pressure below with a large bore plastic syringe and silicone tubing.
can you elaborate?
Vacuum
Equal and opposite 😁😎
Some cheap chemistry equipment , some silicon caulking , gaskets and a cheap walmart vacuum and you will be in business with a capital B in this regard. Not to mention all your friends will be jealous that you can make for 15 bucks what costs them 130 bucks with a GOOD sale going on
umm that's silica gel dude not really sand
We try to use easily understandably terminology so everyone can understand what we are doing, however silica gel is a granular, vitreous, porous form of silicon dioxide and in many parts of the world, silica is the major constituent of sand, but thanks for the constructive criticism, we will take better care of explaining ourselves in the future :)
Thank you very much for showing this I am very interested in this process could you do more videos on this in the bigger equipment. Also besides the colloum what other pieces of equipment are needed for smaller experiments. Again thank you
yo do would you know the ways of making this a basic but still like $100 -$500 set up not even like somthing a one man set up could make some personal CBD from hemp
Endoca CBD 😂
Stfu you pedantic douche bag.
Could you use Activated Carbon instead of sand?
It might decrees the number of times it will need to be filtered.
i love you man! How the hell does this video have 126 haters?
We ask ourselves the same question!
🤔 Any links to your R&D department? There's a cure to the task 😊
But when you say "coffee maker" it opens a pallet of cans of worms 😁 but it is doable.
What if you place sand in the filter of the coffee machine, place gas tube and seal the coffee machine so the pressure can be kept within as much as possible. If the coffee can be assigned for CBD making than you can drill hole for the gas tube to minimize the gas escaping and create the pressure needed. Just was thinking, I am applied chemistry student and I am very interested in the topic of CBD extractions.
Certainly an interesting approach for more diy situations, thanks for sharing!
We put our extraction machinery online here in New Mexico. 50,000 lbs of input material every day. Roughly 2500 kilos of winterized crude production daily. 💪 Distillate to the same capacity by March, 2020.
How long do you leave the solution on the heat source(coffee pad)? What type of container should the solution be in when placed on the heat source?
I can not work out what "liquid" you used in the filtration system, was it ethonal. Iv looked through the comments and you have soaked up all the compliments but havent answered any questions so if anyone knows what liquid he used that would be appreciated
I am wondering if I can take regular gold/brown weed oil and still use this method or do I need to use a full spectrum extract as a start material?
You can use any extract that contains your target material.
Fill water tank of cheap coffee machine with sand, disconnect the heating circuit of the water pre-filter, would the pump then create pressure, evaporate off as usual etc? Great videos man.
Have you guys tried liquid extraction if you did with what solvent? Also curious about what sand is used. Reason for askin, very few people have access to GC equipment to ensure how much thc goes through. Thanx for the video.
The sand we use is a type of silica, and we have done a video on alcohol extraction, however do our extractions at Endoca with C02
i generally use solvent dispersion in a piece of pre washed hemp paper, that's called paper chromatography, and it's based in the different speed of propagation of different compounds trough convection in a solid, you will drop the solution and check the side that countains thc, i don't remember wich side it's, one side will have thc and the other cbd, cut the cbd side, wash the cbd paper with isopropyl alcohol and repeat the process as much as you like, you can buy a fluorsilicon pot in the cooking items in any supermarket, fluorsilicon is shatter proof, to collect the hash in one ball you might want to freeze that.
fss1704 hey I’m looking into making my own CBD crystals and the way you’re explaining it makes sense but would it be possible for you to maybe make a video on the presses and steps you take when doing paper chromatography I think that would help a lot of people like myself who just want to make this at home thank you.
never use isopropanol for anything , people are fucking dumb. do yer homework
Love the videos and that shirt is awesome lol excited to continue following your work :)
Thanks!
I don’t have access to nmr at the moment, and my TLCs are a mess. Wondering what solvent system you’re using and what the r.f. of CBD and THC is for you? I’m running 10% EtOAc/Hexane, but I’m getting some streaking spots.
*Now* you're going after trade secrets lol
Thank for the great video… what size micron sand do u use?
LOVE the fact ur trying to share this info.
In all honesty thou I reakon I've got more chance of sprouting a fanny than than SUCCESSFULLY doing this in the kitchen😂😂
It's definitely not the easiest project to take on, however people had been asking us for a long time how it worked so we thought it was high time we at least tried to explain
I like the attitude of this guy
Thanks!
Thanks for the updated version, how did you apply pressure to the column. Thanks
We are going to check with Henry and get back to you! :)
Henry says he just uses a simple air ballon :)
I have a question on how to make cherry oil. When I was a kid we used to get it all the time but now it's hard to find.
That is an interesting one! Unfortunately we only make CBD products, but I'm sure given enough research online, you can find something.
Can you please make a detail video step by step on how to make crystal 99 percent cbd
You say that for purity you need to pass it through the column multiple times, does that mean you put new sand in the column each time? Otherwise you are passing your clean(er) material through the contamination again or am I missing something?
Great video i love knowledge, maybe this will help a coffee maker the filter chamber isn't sealed, what about using a espresso machine, I'm not sure but I think it has a pressurized chamber. You might consider using something like that.
All the years of school payed off
Not for someone it didn't.
It's 'paid'.
My concern is about the solvant that is used. Is ethanol the solvant used for the industrial / advanced material version ? I thought your company used critical-CO2 for the cbd extraction, as a carrier/solvant ? Is it for the cristals or the oil ?
Hi Celine, nope we only extract using a C02 extraction method. Our previous video just gives people the power to make their own oil at home, if they can't afford to buy it
Hey quick question Dr Smoltry, how much tang you slayin'?
could you make the process automated , using pumps to recirculate the product x number of times need valves and switches but should be able to be done with relay logic no cpu needed just asking i have no clue on viscisity etc
Interesting propostion! 🤓
What kind of liquid
This is great that you share the information
Glad you enjoyed our video!
hi endoca, big fan, loyal customer. still a bit confused how to use my crystals. just ran out of 50mg raw cbd caps and raw oil 150mg so will experiment as i purchased crystals in bulk but never figured out a comparable dose- any advice? my current pain mgmt for crippling rheumatoid arthritis is 10mg raw cbd cap in am, 150mg raw oil-4-6 drops- midday, 50mg raw cbd cap at night and hemp cream hands and elbows... endoca helped me reduce my rx.oxycodone 75% in about 4 weeks... thank you for that. =^..^=
Hi there Kimi! Thank you for your kind words.
If you're interested in experimenting, it really depends on how strong of an oil you want. If you want something close to our formula - it's quite simple: 500mg in 10ml of oil will yield a 5% oil, 1500mg in oil will yield 15% and so forth.
Otherwise, if you like that sort of thing, you can vape the crystals. Here, the dosing is a bit more subjective and it is more up to you how much you add to your vape at one time. If you have any more questions, come on down to our website and feel free to chat with our dedicated care team, who will surely be able to provide you with a lot more information. :)
F
What are you using UNDER the silica to stop it from betting pushed into the valve at the bottom?
This guy and his lab is awesome
We will pass the compliment on to Henry!
You need a tube, some sand, and some liquid? What tube? What kind of sand? What kind of liquid? This video is so damn vague you really didn't tell anything about the process at all, wow! When people make videos like this, it's not to share information but to sell information. Thanks for nothing.
Hey Jessica, you will need chromatography equipment, this is not a video for people to do at home with utensils found around the house. We tried to find a way to do this, but it proved impossible, so we shared with you the basics of how we make our pure CBD, however you will need the appropriate equipment to make it yourself
paper chromatography, google it.
Endoca CBD Jessica is jonesin😂
google "paper chromatography", it's relatively easier and you can do in your home.
i generally use solvent dispersion in a piece of pre washed hemp paper, that's called paper chromatography, and it's based in the different speed of propagation of different compounds trough convection in a solid, you will drop the solution and check the side that countains thc, i don't remember wich side it's, one side will have thc and the other cbd, cut the cbd side, wash the cbd paper with isopropyl alcohol and repeat the process as much as you like, you can buy a fluorsilicon pot in the cooking items in any supermarket, fluorsilicon is shatter proof, to collect the hash in one ball you might want to freeze that.
What sand is used? What is the timing or testing to know when the CBD is through and when the THC is coming.
I have a idea that I believe may work for the coffee pot idea.
Cool vid I really did the shirt though because it is a human right
I dont understand a couple things.
how do you know when the filtering of cbd is done and the thc starts?
does the thc afterwards just get stuck in there and never come out?
I would be scared of getting some thc in the cbd. Can you help me understand this?
Can you clear up what liquid/oil u use as a starting material? Is it CBD oil? Also, any update on the home version of this method?
Yes, its CBD extract and no we don't have an at home method yet
How do you calculate dose strength per weight of material?
Hi I am suffering from depression almost all my life live in England I don't think we can make in house I think it is against the law we have to buy from the shop
It's always better to buy from a reputable source as that way you know exactly what you are getting. Making it at home can be very difficult and the results unpredictable
Couldnt you use a turkey injecter with sand in botton...cofee filter holding in the sand and a weight on top for preasure?
You never say how much pressure you need...espresso maker van get 9 Barre.
That's exactly what I thought! I was looking for this comment. I imagine it would work. What I would do, theoretically, is disable to heating unit (and any alarms the system might have for it like an auto off), putting pure sand in the area for the "puck" of finely ground coffee, then have the machine push it through. Just use a small enough amount to test it and pray it works
You had the right missing info I needed to create some good shit,Ty dude 😎
Welcome!
So you have to start with a cbd Strain or just any strain?
If you want to extract CBD, then a CBD rich strain
Curious if this process works with already been vaped flower (ABV), any thoughts?
Unlikely to have enough cannabinoids left inside to create an end product
Endoca CBD thanks for the reply, I forgot to specify in my query whether this method results in crystals which contain only the Cannabidiol phytocannabinoid, as i understand there are many cannabinoids in flower?
A test tube shaped like a coffee filter? How much pressure? Could an aquarium air pump do it?
will it work if I make cbd butter with organic hemp material ? its off topic I know but I cant seem to find any answers
My thoughts would be if you vaporize the materials at a certain temp, then they liquefy at a lower temp. Now if you you do this temp on the solution at start, then it would liquefy unwanted matter. I believe your hypothesis on the pressure is necessary. My question is you used water as your solvent and slowly added pressure, this eventually would generate heat, as you warm to a certain temp all of the carbon and non crystalline objects would be forced to the bottom. If you are having problems understanding where I am going at this point, research the cubic zarconia creation methods. You have to understand you are working with a crystalline.
So... how would you do it on a coffee machine?
+Rodrigo Delgado take the paper filter and do paper chromatography. No fking equipment nor special solvent needed, just a piece of paper and isopropyl alcohol.
Let me say this, thank God for cannabidiol because it is my medicine as without it my world is too stressful, I feel centered when I use it, 1 dose keeps me going for a week.
Nature's medicine! 🌱
Hi, how much does a big machine cost?
What liquid was in the round bottom flask... if trying to make crystals you could use a ratio of sugar maybe 3:1.... 3 parts marijuana and 1 part sugar water then dehydrate with coffee machine... maybe the THC would crystallize out with sugar..
We have never tried this way, so if you do, let us know how it goes!
Can you freeze precipitate to get the crystals? or just evap?
Not sure, we never tried!
Use a high pressure espresso machine take the heat exchange it into pressure and use that the blow it through the sand
the water distiller has a high limit cut off of 340*F / 171C are there any lost compounds at those temperatures?
#Endoca CBD You got something really good going with this bud. Keep doin' what you're doin' 'cuz the information you give is greatly appreciated. Would be nice if you had a list and/or instructions...along with where can a simple man like myself find something like this for the future? Homemade etc...
Great idea John! We will speak to Henry and see if we can work out some kind of infographic :)
Did u get a response? I’m looking on Amazon for chromatography sets…. Then mix ratios and pressure?
What micron is the sand?
Love this!! Very good.
So glad!
Has he figured out how to create the crystals at home yet ?
Once we have the crystals of CBD, how can I make oils for dog"s intake, do I need to decarboxylate the crystals first?
No, crystals are decarboxylated as they are CBD. We can not give medical advice, even for pets, best to work out what dose your dog needs, it is related to weight and size. Hope that helps!
Does it working With thc?
Where can I buy the machine
Hi. What's the solvent system? Peter
Do you use silica gel in the column?
i think to find out when it stops putting out cbd and starts putting out thc might be a bit tricky
Thin layer chromatography plates to check.
how do you clean your silica between cycles?
Luv your shirt !!!
It's a HUMAN RIGHT indeed !!!
It's a great T-shirt isn't it!
You say that first comes out the cbd. Does the thc eventually comes out or the sand doesn't alloud thc to pass trough. If the thc passes trough when woukd I know its time to get out the destilated liquid to be sure that I only have CBD? Thank you
We use CBD extracts, from our CBD rich hemp plants, therefore we don't actually have THC, or have only very minute amounts which are within the legal limits, in our plant material and therefore our extracts before we get to this point
paper chromatography, i used it a lot to separe the substances in a big page of phun subs, to separe the real substance in the middle of the garbage, i removed the "LCD" from the paper and returned that crap to the seller to sell the unknown shit that was mixed.
Have you looked at an espresso maker to utilize the pressure?
Nope, if you try it let us know how it goes!
Awesome character, would be fun eating some psychedelics with him.
hi I'd like to know how many liters of CBD oil you need to make 1kilo of Pure 99% CBD Crystals ? ? ?
This depends on the strength of your CBD oil as every extract will have varying quantities of CBD inside, so there is no black and white answer to this unfortunately, too many variables involved
Giving weed has an "average" 12% cannabinoid content and assuming you're extracting an indica with 80%CBD by volume, some 8,18% of the mass of the cannabis will be cbd, so if you could theoretically magically without any loss extract 100% of the cbd of the plant to crystals you'd need some 13KG of cannabis per kg of crystal.
How do you filter out sand?
could you let me know what solvent you are putting with the exstract also what is the gas you had in the tank any advese as im tring it to treet my medcal problems thanks for the vid
paper chromatography.
i no that just want to no what solcent for cristals thanks tho
solvents
@@MrHiydrowpeaz pure ethanol is the best choice
Freebase cannabis compounds . Like cbd cocaine
You have to use a classic Espresso machine.
If you try this method and it works for you, let us know!
Please more details which kind of solvent are you using? is there a way do do a good extract at home? so on and so forth i bet here are some more patients that could need this information.
Hey max, we have another video on our channel showing you how to extract your own oil at home here ua-cam.com/video/fYMCA_Tg_vk/v-deo.html this is a video to extract crystals from the CBD extract
Hi! What are you using as movil fase? And what kind of “sand” (I suppose it is silica) ?
Yes it's silica
Hi, what is the liquid solvent used?
thanks
For at-home solvents, we usually recommend using ethanol - the more pure the better, but make sure that it is not a kind of alcohol that is toxic for consumption. After all, the oils and crystals are often ingested. :)
What particle size sand?