MLCCs Palladium and Silver Recovery | No DMG Percipitation

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  • Опубліковано 26 кві 2024
  • A unique way to recover palladium and silver from ceramic capacitors (MMLCCs) with highest yield possible.
    Telecom PCB gold recovery:
    • Telecom PCB gold recov...
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    #palladium
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  • Розваги

КОМЕНТАРІ • 68

  • @PickyPlans
    @PickyPlans  Місяць тому +5

    •Extreme care must be taken while handling platinum group metals.
    • Acetylene gas is a combustible gas and should be Stored and handled far from any open flame.
    • Acids are corrosive and could cause irritation upon contact, should be handled under professional supervision

    • @guytelfer1353
      @guytelfer1353 Місяць тому +1

      I'm doing almost the same thing currently, cool

  • @ayhamhafez285
    @ayhamhafez285 Місяць тому +6

    Great job, don't miss gold, there is also gold in mlcc trust me, also some palladium will not be dissolved in nitric acid but it will be with aqua regia, use AR with undissolved material from nitric bath, then precipitate gold and keep your acid waste into stockpot to get last palladium later. approximately will get 0.3 gram of gold from 1 kg of mlccs

    • @PickyPlans
      @PickyPlans  Місяць тому +3

      Wow that's amazing! I've kept the dross. I'll process it later that's really a high score for gold

    • @lukekingi2210
      @lukekingi2210 Місяць тому

      It's true there is gold, especially in non magnetic mlccs, not much but it is there

    • @PickyPlans
      @PickyPlans  Місяць тому

      Things are getting interesting!

    • @LimbahElektronikIndonesia
      @LimbahElektronikIndonesia Місяць тому

      Mlcc doesn't contain gold.Gold came from tin solder.Especially from gold plated board tin solder.

    • @lukekingi2210
      @lukekingi2210 Місяць тому +1

      @ArieSulistyo-pe2wx the mlccs I process are new old stock (NOS) they have not been soldered to a circuit board

  • @julianalcorso5703
    @julianalcorso5703 Місяць тому

    Another good one Picky!!

  • @Amac-uz9hm
    @Amac-uz9hm Місяць тому

    superb processes great video

  • @aquaregia1672
    @aquaregia1672 Місяць тому

    very nice video thank yolu pickyplans

  • @jamisontaylor878
    @jamisontaylor878 Місяць тому

    Awesome 😊

    • @PickyPlans
      @PickyPlans  Місяць тому

      Thanks for watching 🙏

  • @ImanGoldRecovery
    @ImanGoldRecovery Місяць тому

    excellent video bro 🌹🌹🌹🌹🔥👍

    • @PickyPlans
      @PickyPlans  Місяць тому

      Thank you so much bro🔥

  • @riverboat28
    @riverboat28 Місяць тому

    I'd like to see a closeup of how your using that welder as a torch. Genius....damn dangerous but genius for the smart people.

    • @PickyPlans
      @PickyPlans  Місяць тому

      Sure,I'll cover it in upcoming videos...

  • @user-bi2xp9rx9i
    @user-bi2xp9rx9i День тому

    ساخت بوته خیلی جالب بود👏👏👏

    • @PickyPlans
      @PickyPlans  День тому

      Mamnoon az tavajohe shoma🙏

  • @MiguelSierra
    @MiguelSierra Місяць тому

    muy bien

  • @user-kc6nl9yc7d
    @user-kc6nl9yc7d Місяць тому

    Интересный метод

    • @PickyPlans
      @PickyPlans  Місяць тому +1

      Спасибо, мой друг

  • @alquimiavsmetalica5250
    @alquimiavsmetalica5250 Місяць тому

    I think you are unaware that with this machine you can use it for the electromagnetic coil for an induction oven, it is capable of even melting 316 stainless steel.
    The induction coil will take copper tube and fiberglass jacket, the tube is screwed on a proforma of 2 cm tolerance to the crucible since it needs to be covered with oven concrete.
    To avoid crushing, weld the vehicle chamber valve and plug to the other end and give a little air pump pressure.
    The concrete that covers it is alumina paste but first you have to create a ceramic cloth like a glass for the graphite crucible.
    The uncovered part of the tube is welded fixing for electrical condition and adapter for heat sink with water pump

    • @PickyPlans
      @PickyPlans  Місяць тому

      Thanks mate for the explanation ... If you have the plan send it to my e-mai... Thanks in advance.
      Pickyplans.comm@gmail.com
      By this plan i can just use a silicone carbide crucible i guess also it has a refractory cover as concrete you mentioned

  • @salihakdag6371
    @salihakdag6371 Місяць тому

  • @mehany7462
    @mehany7462 Місяць тому +1

    دستت درد نکنه از بابت زیرنویس فارسی

  • @user-my4xn2wm5u
    @user-my4xn2wm5u 17 днів тому

    مرحبا عمل رائع صديقي اذا تم اطلاق غاز الاسلتين في المحلول هل يرسب نحاس ان وجد ام انه مرسب نقي البلاديوم فقط❤❤❤❤

    • @PickyPlans
      @PickyPlans  17 днів тому

      شكراً جزيلاً. البلاديوم فقط يترسب بغاز الأسيتيلين... النحاس لن يترسب في المحلول الحمضي.. لترسيب النحاس تحتاج إلى محلول قلوي مع الأمونيا ثم يمكنك ترسيبه بالأسيتيلين (لكن كن حذرا أسيتيليد النحاس الذي يتشكل في محلول الأمونيا هو مادة متفجرة) مادة)

  • @enjoybhajan8476
    @enjoybhajan8476 Місяць тому

    Please make video for gold recovery using this method for ic

    • @PickyPlans
      @PickyPlans  Місяць тому

      Good idea. I intended to do this method + copper cell electrolysis to get gold .
      Since i think there is no point in using nitric acid after this method.

  • @2001pulsar
    @2001pulsar Місяць тому

    I got 2.4g per 300g resin dip MLCC.
    From just smelting in different fluxes with silver and lead collector

    • @PickyPlans
      @PickyPlans  Місяць тому

      Great job and yield data... Did you use borax and sodium carbonate as flux?

    • @2001pulsar
      @2001pulsar Місяць тому +1

      @@PickyPlans borax and nitrate initially to destroy the resins and some base metals, then borax and caustic to dissolve the ceramic substrates. After the second smelt, the slag was nice and glassy and the metal button was clean and separated from the slag easily.

    • @PickyPlans
      @PickyPlans  Місяць тому

      Great aproach! Thanks 👍

  • @erfanhashemi5177
    @erfanhashemi5177 Місяць тому

    عالی 👏

  • @user-vi8hx3xs9l
    @user-vi8hx3xs9l Місяць тому

    God bless you, a very wonderful job, can I know what material you deposited in silver with the details if you honor 20:11 20:11

    • @PickyPlans
      @PickyPlans  Місяць тому

      Thank you my friend.
      First i used HCl to drop silver chloride then i filtered and washed it then 3 table spoons sodium hydroxide added and stirred to get fully black material then 2 table spoons of sugar added and let to react... Your silver powder is ready to wash and melt

  • @CatboyChemicalSociety
    @CatboyChemicalSociety Місяць тому

    Wouldn't this risk forming acetylides with other metallic solutions which are dangerous explosives

    • @PickyPlans
      @PickyPlans  Місяць тому +1

      Not at all! As i mentioned in the video (silver and copper carbide or acetylides) When you precipitate silver as chloride beforehand silver could not make acetylide in next steps and copper needs to be reduced to Cu+ in ammoniacal solution (using reducing agents like hydroxylamine) .it would not form acetylide in acidic condition at all
      -Red blood color (Copper acetylide/carbide)
      -white gray color (Silver acetylide/Carbide).
      I used the "energetic" word instead of explosive in the video.
      And other metals carbide/acetylide are not explosives like palladium carbide we recovered or tungsten carbide used as hard material to make cutting tools.

    • @CatboyChemicalSociety
      @CatboyChemicalSociety Місяць тому

      @@PickyPlans will this seperately precipitate Pd from other pgms like Ru, Ir, Pt and Os

    • @PickyPlans
      @PickyPlans  Місяць тому +1

      No Acetylene would react the same with other PGMs. You need to use other methods to separate PGMs (using ammonium chloride to get platinum and iridium out . Then cement remaining PGMs using zinc fuse the mix metals with sodium Bisulfate to make rhodium soluble in water (as ion) then process for rest of metals by doing Alkaline fusion (NaOH and KNO3 mix)
      But you really need to be careful about osmium.

    • @asdwee4444
      @asdwee4444 Місяць тому

      @@PickyPlans Why be careful with osmium ?

    • @PickyPlans
      @PickyPlans  Місяць тому +3

      Upon heating in air( or smelting with alkali )it turns into Osmium Tetroxide which boils at 40 ° C It reacts with the retinol in your eyes and blinds you

  • @zafarazmi7599
    @zafarazmi7599 Місяць тому

    ❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤❤ very good 👍

  • @user-yu5ol5vz7q
    @user-yu5ol5vz7q 22 дні тому

    Шото совсем мало ПД🤔👍

  • @user-zm7sy8sy3j
    @user-zm7sy8sy3j Місяць тому

    عالی

  • @CB-68-westcreations
    @CB-68-westcreations Місяць тому

    I'm surprised you got away with using a carbon ark to melt platinum group metals. Since platinum likes to soak up carbon

    • @PickyPlans
      @PickyPlans  Місяць тому +2

      The graphite rod didn't touch the molten charge, I placed it on the top but it was very close to the charge. The arc would lean into the charge at a certain distance of electrodes.

  • @quinton3997
    @quinton3997 22 дні тому +1

    Not very much palladium

    • @PickyPlans
      @PickyPlans  21 день тому

      Only old and not magnetic worth processing

  • @casilyas1985
    @casilyas1985 Місяць тому

    500 gr mlc = 0.66 gram palladium 😞😓😩😫😭👍👍👍👍👍

    • @PickyPlans
      @PickyPlans  Місяць тому +2

      Unfortunately yes. Of course it depends on the year of manufacture it could be higher.

    • @casilyas1985
      @casilyas1985 Місяць тому +1

      You are a very good master, the video is super​@@PickyPlans

    • @PickyPlans
      @PickyPlans  Місяць тому +1

      @casilyas1985 Thank you, I appreciate your kind words.

  • @user-vj6qz2uk2u
    @user-vj6qz2uk2u Місяць тому

    Не доплатил .Нужно индуцционую печь .Температура 1450 градусов

    • @PickyPlans
      @PickyPlans  Місяць тому

      Да и индукционная печь с тиглем из карбида кремния отлично подходит для такого материала

  • @FollowMe2aMillion
    @FollowMe2aMillion Місяць тому

    Loving your videos friend.