Hi Nawaz, the video has soothing music with calm explanatory movements. Today first time I got this to watch, Its of immensely valuable for me. Query: d-spacing I calculated, its different for different planes, thus do we need to report its average value in manuscript. else please help me which d-spacing value we need to consider. Eagerly awaiting for your response.
I thank you for your eminent work. I would like to clarify a few. How to find the corresponding plane hkl value for these calculated d spacing? For example, if I have d spacing as 2.3 A, whether it corresponds to plane 001?
Haha, I am also looking for an answer to this question. It seems that the interplanar spacing related to the Miller index is different from here, but I don’t know how they are related. For example, I want to know the crystal structure of a crystal (020) belonging to the monoclinic system. Do I calculate the distance between faces by d=nl/2sin(Theta)? Or is it calculated by dhkl=1/sinβ2*(h2/a2+l2/c2+2hlcosβ/ac+k2*sinβ/b2)?
Hello, the is video is very helpful, I followed the same, it is showing me that "Fit did not converge - mutual dependency exists between parameters. You may have overparameterized the fitting function. Fixing one of them may eliminate this problem". how to resolve
hello thank you very much for your effort. You are doing appreciable job. I would like to ask that the d spacing values corresponding each peak you found are different so for such an analysis what would be the number for d spacing at last? I mean will we get the average value or not ? I am looking forward to hearing from you
Thank you for your excellent video. As there is a d-spacing value for each peak, and they are different from each other. So when reporting the d-spacing value we should mention the corresponding peak. Is this right? If not, how can we determine the exact d-spacing value? Many thanks.
I have another version of the Origin Program I could not follow your steps, I dont have the same menu on the program, if I send my x-uy data cold you calculate the d-space for me? of teta? highly appreciated
Thanks for your amazing videos. I have a question for you, my highscore software doe not work "search peak", so I cant continue the next steps, is there any setting for software to active ''search peak''?
Thanks for informative tutorial, i am new to the research kindly guide me what can be done if peak fitting is not perfect??
Your all videos are much appreciated. Please keep the work up. Thanks.
Hi Nawaz, the video has soothing music with calm explanatory movements. Today first time I got this to watch, Its of immensely valuable for me. Query: d-spacing I calculated, its different for different planes, thus do we need to report its average value in manuscript. else please help me which d-spacing value we need to consider. Eagerly awaiting for your response.
Thanks a lot for providing me software and helping me in my XRD data
Deep gratitude for helping me a lot
I thank you for your eminent work. I would like to clarify a few. How to find the corresponding plane hkl value for these calculated d spacing? For example, if I have d spacing as 2.3 A, whether it corresponds to plane 001?
Haha, I am also looking for an answer to this question. It seems that the interplanar spacing related to the Miller index is different from here, but I don’t know how they are related. For example, I want to know the crystal structure of a crystal (020) belonging to the monoclinic system. Do I calculate the distance between faces by d=nl/2sin(Theta)? Or is it calculated by dhkl=1/sinβ2*(h2/a2+l2/c2+2hlcosβ/ac+k2*sinβ/b2)?
Hello, the is video is very helpful, I followed the same, it is showing me that "Fit did not converge - mutual dependency exists between parameters.
You may have overparameterized the fitting function. Fixing one of them may eliminate this problem". how to resolve
Thank you very much, this helped me a lot!
Glad it helped!
hello thank you very much for your effort. You are doing appreciable job. I would like to ask that the d spacing values corresponding each peak you found are different so for such an analysis what would be the number for d spacing at last? I mean will we get the average value or not ? I am looking forward to hearing from you
check your email
Same question for me also sir. Pls reply
Hi..if u got your answer, please tell me how we get the single exact value? by average?
How is it known the diffraction order is 1? Is it not different for different peaks?
Obrigado por este video. Estou trabalhando com difração de raios X. Atuando exatamente nesta área de distancia inter planar.
This video might be helpful for you.
What if peaks are not fitted well?
Thank you for your excellent video. As there is a d-spacing value for each peak, and they are different from each other. So when reporting the d-spacing value we should mention the corresponding peak. Is this right? If not, how can we determine the exact d-spacing value? Many thanks.
Hi, nice video I have got a overview about how to calculate d space value... I have small doubt.. How to convert d space value in nanometer.
Just divide your d-spacing value in Angstrons by 10. The relationship is 1 nm = 10 Â
I have another version of the Origin Program I could not follow your steps, I dont have the same menu on the program, if I send my x-uy data cold you calculate the d-space for me? of teta? highly appreciated
sir, how we get values of wavelength & order of diffraction? , which value we will use?
Thanks for your amazing videos. I have a question for you, my highscore software doe not work "search peak", so I cant continue the next steps, is there any setting for software to active ''search peak''?
It should, What version you are using?
Why its showing "Fit did not converge. Maximum iteration setting of 400 was reached" in my peaks? How can I correct It?
I am getting some negative values for d-spacing, is that allowed?
keep on doing this video
Thank you so much
Muchas gracias, eres el mejor
thank youuuuu
Good
Thank you sir
Welcome
Thank u sir
What to do if fit did not coverage?
then fit each peach individually (one by one)