hello friend could you oxidice toluene to benzaldehyde by electrolysis with potassium ammonium persulfate? In the third season of hamilton pharmacopea, the mythical uncle fester is interviewed and the method is shown, it seems very easy and has the advantage that it is very cheap, it does not pollute or is carcinogenic like our friend chromil chloride. The metod is electrolisis
If you have a link to the preparation I can for sure try it given that potassium ammonium persulfate can be switched out with ammonium or sodium persulfate.
@@THYZOID here’s video, synthesis starts at around first minute: ua-cam.com/video/rDvPrRQjd58/v-deo.html . Though, I’ve heard that many “easy” methods from Uncle Fester’s books only provide food for thought and don’t work in practice, and probably this is the case for this particular show about drugs
@@tolyan9756 Hi friend.. The reactions are well explained and you can also see the steps, although for me the translation into Spanish is a bit difficult. note: let's see if our friend illustrates the reactions in a new video of THYZOID LABORATORIES. Gracias por escribirme👍
@@THYZOID hey!! If you ever make a video on the chromyl chloride test, will you mention my channel and will you pls put a link down in the description, coz getting proffessional mention for an amateaur chemist is very rare!!
Cont: both attempts at making my own ampules flunked out! So now I have been preparing for my chromyl chloride synthesis for the past 4 months now ( buying the proper equipment and supplies) but I really cant find any empty ampules for sale, so I purchased 30ml ulab test tubes with the bakelite and teflon screw cap, hoping I can store it in there. Any feedback would be oh so great on this conundrum! Thank you all!
I bought two heavy bottles of battery acid recently just incase I couldn't buy it again. 15% would seem about right though. Every 1000ml I distil I get 100ml concentrated acid at the end plus a weaker fraction before it and of course lots of water
Where in Gods name did you get the ampules from? Or did you just make them from test tubes? I have tried to make a couple ampules using test tubes and a propane torch but I think the glass was a bit too thick as I had the propane torch at full blast but it took forever to start to soften up, then crack city man! All went to hell both times!
Thy Labs: chromyl chloride is dangerous so i will wear a gas mask Nile Red: Chromyl chloride is fun to play with, and one of my favorite chemicals Me: all liquid is drink. me drink red juice now
Wie regelst du eigentlich das rechtliche bei deinen Versuchen? In dem Video benutzt du ja konzentrierte Schwefelsäure, die für Privatpersonen nicht erlaubt ist.
Hey man to get rid of any contaminants that are in the chromyl chloride in the final product I was thinking about using DCM to dissolve it and then boil the DCM would that work do you think ?
@@SizzlyPK The fact that you asked this question is very concerning, I wouldn't try and make chromyl chloride until you are very confident and know the answers to questions like these first!
Why are the most dangerous chemicals and elements almost always the most beautiful? Bromine, Mercury, Chromyl Chloride, Chlorine, Actinium, the list goes on...
so, if this is the last year where sulfuric acid can be used due to the EU regulations, after it passes, are you gonna get rid of all the acid and never use it again?
It’s more than 75 liters of diluted acid in its entirety. 60 l diluted in water, 15l in other mediums. Gotta stock up for an entire life. It’s legal so the gov shouldn’t have a problem and if they do I don’t give a damn because it’s totally legal.
@@THYZOID I would think only if you're BUYING it higher than that, from a store or someone, or selling it, it would need to be lower than 15%. Who will come to your house to make sure your acid is 15% or lower ? I wonder if you can buy car battery acid solution there, as most of it is 35% in concentration. They can't just decrease the concentration for batteries, so then they should also ban lead acid batteries, anyone can open a car battery and get a higher concentration anyways... Precursors to sulfuric acid are available, in the worse case you can concentrate your weak acid.
@@Ryan-lc4bl for batteries there is a special law and only “professionals“ (people with a license) are allowed to refill it… it actually applies not only to sales but it extends to mere possession. I’m not going to risk it as there are plenty of (highly dangerous) alternatives to sulfuric acid.
0:10 "do not try to make chromyl chloride neither at home nor in the lab. welcome back everyone, today we are gonna make chromyl chloride"
Hell yea! Chromyl Chloride is such a beautiful compound, though my lungs would certainly disagree. Lovely video!
Cromyl chloride is my favourite compoynd because it can oxidise toluol to benzaldechide.
Very interesting compound, nice reactions!
Ascorbinsäure acid ^^ 0:24
Hab’s schon gesehen^^
Das ist mir sogar durch das zweite mal bearbeiten gerutscht
Already noticed it^^
I oversaw it even after the second edit
Wollt ich auch grad schreiben
I'm wondering if there is a similar compound made from molybdenum, since it's the only other hexavalent element?
hello friend could you oxidice toluene to benzaldehyde by electrolysis with potassium ammonium persulfate?
In the third season of hamilton pharmacopea, the mythical uncle fester is interviewed and the method is shown, it seems very easy and has the advantage that it is very cheap, it does not pollute or is carcinogenic like our friend chromil chloride. The metod is electrolisis
If you have a link to the preparation I can for sure try it given that potassium ammonium persulfate can be switched out with ammonium or sodium persulfate.
@@THYZOID ua-cam.com/video/rDvPrRQjd58/v-deo.html
@@THYZOID here’s video, synthesis starts at around first minute: ua-cam.com/video/rDvPrRQjd58/v-deo.html . Though, I’ve heard that many “easy” methods from Uncle Fester’s books only provide food for thought and don’t work in practice, and probably this is the case for this particular show about drugs
@@tolyan9756
Hi friend.. The reactions are well explained and you can also see the steps, although for me the translation into Spanish is a bit difficult. note: let's see if our friend illustrates the reactions in a new video of THYZOID LABORATORIES.
Gracias por escribirme👍
Why don't you have a patreon? I would definitely sign up.
That’s a great idea I’m going to look into soon! Just took a screenshot in order not to forget it^^
Mans unhinged absolutely no fear
Nile red reference
Why didn't you make the chromyl chloride directly from hcl and the chromium trioxide
Hard to mix them in a blender ☺
Seriously: HCl is mostly water, which destroys the product.
Chromium trioxide is more expensive. Besides that gaseous HCl must still be used and therefore it wouldn’t have been easier.
@@THYZOID ah thx
Why is this the last year you can use concentrated sulfuric acid?
Possesion of sulfuric acid above 15% will be illegal in the EU after febuary 2022. It's very unfortunate for amateur chemists in Europe.
This^
Can i also dry Sodium sulfate decahydrate in the microwave?
Scary Chromyl chloride potentially causing cancer with prololonged exposure. Are you going to reduce organic material with it?
Any recommendation? I don’t have an actual plan on what to do with it at the moment.
@@THYZOID plan a video on the chromyl chloride test for chloride ions and tell us how the test works!!
Sure!
@@THYZOID ✌✌
@@THYZOID hey!! If you ever make a video on the chromyl chloride test, will you mention my channel and will you pls put a link down in the description, coz getting proffessional mention for an amateaur chemist is very rare!!
Cont: both attempts at making my own ampules flunked out! So now I have been preparing for my chromyl chloride synthesis for the past 4 months now ( buying the proper equipment and supplies) but I really cant find any empty ampules for sale, so I purchased 30ml ulab test tubes with the bakelite and teflon screw cap, hoping I can store it in there. Any feedback would be oh so great on this conundrum! Thank you all!
Similar like bromine
Ouch pretty hard to do anything without sulfuric acid. Did they just ban it in the EU?
they banned H2SO4 >15%
I bought two heavy bottles of battery acid recently just incase I couldn't buy it again. 15% would seem about right though. Every 1000ml I distil I get 100ml concentrated acid at the end plus a weaker fraction before it and of course lots of water
Huh, never heard a magnetic stir bar called a "stir fish" before but that's a neat name :D
In Germany it's often called a "Rührfisch"
Where in Gods name did you get the ampules from? Or did you just make them from test tubes? I have tried to make a couple ampules using test tubes and a propane torch but I think the glass was a bit too thick as I had the propane torch at full blast but it took forever to start to soften up, then crack city man! All went to hell both times!
Got them from a nearby lab shop
Huh, really very interesting compound 😍
Thy Labs: chromyl chloride is dangerous so i will wear a gas mask
Nile Red: Chromyl chloride is fun to play with, and one of my favorite chemicals
Me: all liquid is drink. me drink red juice now
Mildred now: does glove chemistry and nothing even remotely dangerous
stir-fish? ok that's fun
Wie regelst du eigentlich das rechtliche bei deinen Versuchen? In dem Video benutzt du ja konzentrierte Schwefelsäure, die für Privatpersonen nicht erlaubt ist.
checke das uploaddatum.... mittlerweile dürfte ich als geschäftskunde aber auch wieder konz H2SO4 kaufen
@@THYZOID Danke für die schnelle Antwort. Das Datum hatte ich übersehen. Ist ja auch eine relativ neue Regelung
Come to America, Friend, we don't have a ban on sulfuric acid :)
You may not have a ban on sulfuric and nitric acid but a lot of other reagents that are nearly otc here cannot be bought easily….
@@THYZOID why are those acids banned now?
Ask the politicians who banned them
@@THYZOID I could have sworn it was because of rising acid attacks?
“For public safety because think about the children“
Hey man to get rid of any contaminants that are in the chromyl chloride in the final product I was thinking about using DCM to dissolve it and then boil the DCM would that work do you think ?
if you just dissolve in dcm followed by boiling it off you wouldn´t accomplish anything. just distill the chromyl chloride
@@THYZOID okay thank you
@@SizzlyPK The fact that you asked this question is very concerning, I wouldn't try and make chromyl chloride until you are very confident and know the answers to questions like these first!
Wie heißen diese roten ,, Muffen“ um den Kühler mit den Schläuchen zu verbinden ?
keck klemmen
Why are the most dangerous chemicals and elements almost always the most beautiful? Bromine, Mercury, Chromyl Chloride, Chlorine, Actinium, the list goes on...
And what's that Ascorbinsäure acid?
this was autocorrect. It´s just ascorbic acid
Muy bueno
Yeah!!...."Fun" properties...
your blood doesnt fume? weird
cool
so, if this is the last year where sulfuric acid can be used due to the EU regulations, after it passes, are you gonna get rid of all the acid and never use it again?
I am diluting it down to
@@THYZOID should work, but then again, 15 liters of acid is still a bit sussy
It’s more than 75 liters of diluted acid in its entirety. 60 l diluted in water, 15l in other mediums. Gotta stock up for an entire life. It’s legal so the gov shouldn’t have a problem and if they do I don’t give a damn because it’s totally legal.
@@THYZOID
I would think only if you're BUYING it higher than that, from a store or someone, or selling it, it would need to be lower than 15%.
Who will come to your house to make sure your acid is 15% or lower ?
I wonder if you can buy car battery acid solution there, as most of it is 35% in concentration. They can't just decrease the concentration for batteries, so then they should also ban lead acid batteries, anyone can open a car battery and get a higher concentration anyways...
Precursors to sulfuric acid are available, in the worse case you can concentrate your weak acid.
@@Ryan-lc4bl for batteries there is a special law and only “professionals“ (people with a license) are allowed to refill it… it actually applies not only to sales but it extends to mere possession. I’m not going to risk it as there are plenty of (highly dangerous) alternatives to sulfuric acid.
next video how to make amphetamine pls
jk :)) nice video, you have a cool channel, I'm here from the reddit post.
Appreciate it! I won’t do anything illegal though
Cancer juice 😂😂😂
0:37 Ascorbinsäure acid?!?! Oops, at this moment German broke through. 😊😂😂😂
autocorrect.....
Yum
Baby food 😋
Schöne Synthese! Manchmal hörst du dich aber leider auch etwas gelangweilt an, wenn du redest :-) .
Passiert ab und zu wenn ich morgens die Videos bearbeite 😂
Mix it with hydrazine
maybe then the test tube becomes a rocket XD
Thy Labs 🧪 saves the most exciting chemical reaction for last!