Nitrosyl perchlorate - Mixed anhydride of Nitrous and Perchloric acids

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  • Опубліковано 13 жов 2024

КОМЕНТАРІ • 119

  • @thetrashman42069
    @thetrashman42069 2 дні тому +79

    this channel is so incredibly underrated, these kinds of videos deserve millions of views

    • @josephodle1660
      @josephodle1660 2 дні тому +3

      Fully

    • @ChemicalForce
      @ChemicalForce  День тому +7

      🥲

    • @thetrashman42069
      @thetrashman42069 День тому +2

      ​@@ChemicalForceone of these days the algorithm will start recommending your videos and you'll get the recognition you deserve

    • @scrappydoo7887
      @scrappydoo7887 День тому

      @@thetrashman42069 yup you're spot on

  • @ZoonCrypticon
    @ZoonCrypticon 2 дні тому +31

    The problem with chemicals is always waste disposal, cleaning up the mess afterwards, storage of the chemicals, safety hazards. That´s the reason, why I am grateful to you, that I can watch your videos from the warmth of my home.

    • @naderabyad1722
      @naderabyad1722 День тому +6

      He doesn't need to clean any glassware... New glassware for each project

    • @sprolyborn2554
      @sprolyborn2554 День тому +6

      you mean you dont just dump your spent chemicals straight into the ocean? boy have i been doing it wrong!

    • @ChemicalForce
      @ChemicalForce  День тому +11

      @@naderabyad1722 New lab for each project!

    • @LesNewell
      @LesNewell День тому

      @@ChemicalForce This time I want 1/2" thick glass in my fume hood!

  • @spiderdude2099
    @spiderdude2099 2 дні тому +7

    The blue nitrous acid color is so pretty

  • @nocturnhabeo
    @nocturnhabeo 3 дні тому +54

    I feel like a lot of the hazard stuff is done once and recorded and everyone else was like "w/e man I don't need to check, I like my hands/eyes/parts where they are"

    • @belacickekl7579
      @belacickekl7579 2 дні тому +4

      "Hmm, perhaps the author was making stuff up when he described the yield percentage of chlorine azide! I'll just get my blast shield and go double-check that"
      said no chemist ever.

    • @christopherleubner6633
      @christopherleubner6633 День тому +1

      Yup, let's use the MSDS as a challenge speed run. 😂

  • @AJ-qv9yo
    @AJ-qv9yo 2 дні тому +9

    Brutal stuff. When CF says "it’s a bad sign," you know things are about to get intense. Honestly, I’m just relieved I’m not his neighbor... haha. This channel is pure gold. CF tackles the wildest experiments so the rest of us can sit back and watch. And the fact that it's all captured with such pro-level filming? Incredible. Though I can’t imagine how fun it must be to clean up the lab after all that madness!

  • @nuneke0
    @nuneke0 2 дні тому +8

    Wow! The high-speed footage never disappoints!

  • @peterteatree
    @peterteatree День тому +2

    That borane reaction looks like true “magical alchemy” 😮

  • @drhxa
    @drhxa 16 годин тому +1

    Wow I've never seen two solids in direct contact react without adding any heat. Nice

  • @SuperAngelofglory
    @SuperAngelofglory 2 дні тому +13

    Nitrosyl perchlorate bigger brother, nitronium perchlorate, also exists and it is even more spirited. Can be made by mixing 3 gases:
    NO2+ClO2+2O3 = NO2ClO4 + 2O2.
    Was intended for use in rockery in the 1950s, but eventually they gave up, as it was too unstable for that!

    • @dapossum9495
      @dapossum9495 День тому +5

      Apparently, it can also be made by bubbling nitryl chloride through a silver perchlorate solution in nitromethane. Silver chloride will precipitate and can be filtered out, leaving a solution of nitronium perchlorate in nitromethane.

    • @SuperAngelofglory
      @SuperAngelofglory День тому +4

      @@dapossum9495 am I crazy for wanting to ignite such a solution?

    • @cezarcatalin1406
      @cezarcatalin1406 День тому +2

      you can also oxidise nitrosyl perchlorate directly with ozone

    • @ChemicalForce
      @ChemicalForce  День тому +6

      ​@@cezarcatalin1406 Literally two days ago I tried passing ozonated oxygen through liquid nitrosyl chloride, but no reaction occurred. Perhaps much more concentrated ozone is needed here 🤔

    • @dennisford2000
      @dennisford2000 День тому

      @@dapossum9495so now do you attempt to separate them? If so how, and how dangerous is that. Sounds like a good idea to be a couple miles away….

  • @jimsvideos7201
    @jimsvideos7201 2 дні тому +7

    That blue colour off the first reaction was pretty.

    • @naderabyad1722
      @naderabyad1722 День тому

      It seems like a transition metal ion is present in solution...

  • @sulaimanabdullah952
    @sulaimanabdullah952 2 дні тому +1

    Thanks for your excellent videos.
    Intro, reactions,photography,lighting,sound tracks, wow!!

  • @InternetFiend68
    @InternetFiend68 День тому +1

    This channel is incredibly underrated...

  • @erictjones
    @erictjones 2 дні тому

    Yet another great video with visually stunning reactions in slow motion. Bravo!

  • @scrappydoo7887
    @scrappydoo7887 2 дні тому +2

    I love this channel.
    I wish more creators had the kit and chemicals available to make these reactions

  • @scrappydoo7887
    @scrappydoo7887 2 дні тому +2

    The high speed shots are beautiful btw 🙂

  • @dominicestebanrice7460
    @dominicestebanrice7460 День тому

    Mesmerizing visuals: bravo!

  • @RafaCB0987
    @RafaCB0987 2 дні тому +1

    Those explosions were realy beutiful on slow motion

  • @fredkow553
    @fredkow553 День тому +1

    aprecio mucho la calidad de este canal, no hay nada igual

  • @yugbe
    @yugbe 2 дні тому +1

    I love this channel!!

  • @aupotter2584
    @aupotter2584 2 дні тому +2

    I agreed that handbook and even labelled hazardous symbols can be misleading if not entirely wrong. I'd ever disposed of an old but unopened bottle of triphenylamine with the aid of a lab technician. The bottle was well sealed and wrapped with Teflon jacket and then put inside a box, but the label simply said 'harmful' only, but what I know is that tertiary aromatic amine is quite toxic instead. My lab tech wore a wrong pair of plastic gloves and some amine poured oozed through the glove, causing skin absorption of the chemical. Luckily, he's still alive, but I can't forget its smell of roasted dried squid, which I'll never dare to eat since then.

    • @hantrio4327
      @hantrio4327 День тому

      Triphenylamine is not dangerous. It has no GHS pictograms

  • @ormarion552
    @ormarion552 2 дні тому +2

    im curious how the reaction of it with anhydrous hydrazine would have been if you dropped the solid onto the hydrazine into a test tube. In any case that was super cool, never heard of this compound before

  • @theprof73
    @theprof73 День тому

    Let's do all the things in this book of things you aren't supposed to do. I love it.

  • @scottybadmoon3857
    @scottybadmoon3857 День тому

    Thank you... I should have studied chemistry years ago.1st yr atm. Wild class...yes sir. 😊Cheer's

  • @rogerpentagon
    @rogerpentagon День тому

    Love your work. ❤ Thank you.

  • @ashe1.070
    @ashe1.070 День тому

    Neat! I’ve never heard of this compound. Can you try this again with nitromethane, 2-nitropropane, carbon disulfide, and solutions of various reagents like butyl lithium, sodium borohydride, lithium aluminum hydride, etc.? Maybe even with diazomethane, dimethyl zinc (or diethyl zinc), and trimethylaluminum. The results would be very interesting to see.

  • @janf1174
    @janf1174 2 дні тому +1

    Really cool slomos

  • @matze1389
    @matze1389 2 дні тому +1

    Seconds😮 LOVE your videos

  • @raylam4637
    @raylam4637 День тому

    Incredible🎉, amazing

  • @Grateful.For.Everything
    @Grateful.For.Everything День тому

    ❤️ Incredible

  • @Чженьцзю-й2д
    @Чженьцзю-й2д 9 годин тому

    Прекрасное видео, давно ждал!!!
    Думаю, следующее видео будет с перхлоратом нитрония NO2(ClO4) - синтез, реакции, растворение в C(NO3)4 и взаимодействие этого раствора с другими веществами.

  • @j_sum1
    @j_sum1 День тому

    That looks like an awesome book.

  • @Willrocs
    @Willrocs 2 дні тому

    Thanks for these vids.

  • @APolitically
    @APolitically День тому +2

    Please also do Nitronium Perchlorate!

  • @Pennie7077
    @Pennie7077 2 дні тому +3

    Cool! Nitronium tetrafluoroborate when?

    • @blattgruener1216
      @blattgruener1216 2 дні тому +4

      true he said in a previous Video that "it is to exotic for this channel - for now" (if i remember correctly) has been 3 Years so lets see it :)

    • @Pennie7077
      @Pennie7077 2 дні тому

      @@blattgruener1216 liquid boron trifluoride maybe really exotic (A mixture of liquid boron trifluoride and liquid hydrogen fluoride is required for synthesis)

    • @ChemicalForce
      @ChemicalForce  День тому +3

      @@blattgruener1216 it's true! 💯😀

  • @jpolowin0
    @jpolowin0 2 дні тому

    The differences between your observations and the literature (combustion vs. explosion) might depend on reaction conditions: amounts, temperature, which substance is added to the other. Thank you for doing these experiments and showing us the results! I'd be interested in seeing the behaviour of the various nitrogen halides... if you're willing to chance even those dangerous compounds. After all, it would be instructive to _show_ people why mixing bleach and ammonia is a bad idea.

  • @Rehbet
    @Rehbet День тому

    I'd love to see more solid on solid reactions

  • @matsm0n0
    @matsm0n0 День тому

    Nice video. Do you think it would be correct to assume the explosions that occurred when mixed with the solvents were due to the auto-ignition temperatures of the fluids? Once that temperature is reached, the reaction has already vaporized enough of the solvent to cause an explosion in the gases present.

  • @jansz1589
    @jansz1589 День тому

    Would it be possible for you to link those papers in description to give us the ability to examine them in more detail?

  • @madmattdigs9518
    @madmattdigs9518 2 дні тому

    That was cool.

  • @makylemur7019
    @makylemur7019 2 дні тому +1

    Source: Bretherick's Handbook of Reactive Chemical Hazards.

  • @christopherleubner6633
    @christopherleubner6633 День тому +1

    MSDS: This chemical is extremely hazardous when mixed with this one. Don't do it, you might 💀
    Chemical Force: 🤔 Here hold my beaker. 😅😅😅

  • @moocow4749
    @moocow4749 2 дні тому

    Whats the soundtrack for the first two minutes of the video? Love the reactions!

  • @1HeartCell
    @1HeartCell 2 дні тому

    Did they specify how they performed the contact-experiments? It would be a difference if you drop ethanol onto something, or throw the stuff into it.

  • @Labhamsterua
    @Labhamsterua День тому

    You've already made video about NOCLO4

  • @yahyae3416
    @yahyae3416 День тому

    I want sulfuryl chloride experiments

  • @Kargoneth
    @Kargoneth День тому +1

    Chlorine gas, oxygen gas, and nitrogen dioxide are the decomposition products? Yikes!
    What could *possibly* go wrong?

    • @Kargoneth
      @Kargoneth День тому

      That was a rhetorical question.

  • @BigParadox
    @BigParadox 2 дні тому +1

    Whenever a new video comes out from this channel, I watch it immediately! That is not true for any other channel I subscribe to.

    • @scrappydoo7887
      @scrappydoo7887 День тому +1

      @@BigParadox the only other I do it for is explosions&fire2 👍

  • @AJ-qv9yo
    @AJ-qv9yo 2 дні тому

    What is the soundtrack of the borane experiment. BTW, only technical grade? I am disappointed.... :D

    • @AJ-qv9yo
      @AJ-qv9yo 2 дні тому

      found it: The Mill, Marten Moses

  • @swjatt
    @swjatt 2 дні тому

    you are awesome)

  • @IVideo-fc1ng
    @IVideo-fc1ng День тому

    👍

  • @f800gt76
    @f800gt76 2 дні тому

    I've waited for a final boss - decaborane-14 ))

  • @Gajsu1
    @Gajsu1 2 дні тому

    It it possible for you to synthesise noble gases compounds, by that i mean mostly Xe compounds? I've never seen one anywhere.

    • @hantrio4327
      @hantrio4327 День тому

      I don't think so. You need fluorine for that. He would have already made a video about fluorine I he would be comfortable using it (I don't count the one with metal fluorides because the amount was so little)

    • @cezarcatalin1406
      @cezarcatalin1406 День тому +1

      @@hantrio4327
      you can technically use chlorine
      a mixture of oxygen, chlorine and xenon ionised with microwaves forms xenon chlorides
      those chlorides can be absorbed into a sulfuric acid bath below where XeO2 forms initially then it disproportionates to XeO3
      XeO3 can react with Ba(OH)2 to form Ba(HXeO4)2 and then disproportionate into BaXeO6.
      This can turn to other perxenates.

    • @hantrio4327
      @hantrio4327 День тому

      @@cezarcatalin1406 never heard of xenon chlorine compounds. They seem even less stable. I still don't think he will do it. Too complicated of a synthesis. Maybe he will buy some for a video one day but I think he will first explore many other exotic compounds

  • @mcwolfbeast
    @mcwolfbeast День тому

    Definitely one of the more angry chemicals around :P

  • @IcarusSpeaks
    @IcarusSpeaks 2 дні тому +1

    It's crazy how two dry powders can simply touch and react without any other influence.

  • @eeshtarr
    @eeshtarr День тому

    Isn't the color of HNO2 in water actually N2O3 being in equilibrium?

  • @Esterified80
    @Esterified80 День тому

    Try it with white phosphorus and alkali metals

  • @JohnLeePettimoreIII
    @JohnLeePettimoreIII 2 дні тому

    one more chemical to add to my *_"Nope List"._*

  • @psychoabhi2618
    @psychoabhi2618 2 дні тому

    I have a question how to separate sodium chlorate from sodium chloride solution

  • @Ratzfourtyfour
    @Ratzfourtyfour 2 дні тому

    Let's verify all information in that book.

  • @debrainwasher
    @debrainwasher День тому +2

    Acetone with an unstable perchlorate? Great! Just my sense of humor. More fun is only provided by acetone mixed with hydrogen peroxide in an ice bath and seasoned with a tiny bit of citric acid - as a catalyst. Please don't try this at home.

    • @Paonporteur
      @Paonporteur День тому +1

      Citric acid would suffice? Ça m'étonne

    • @scrappydoo7887
      @scrappydoo7887 День тому

      @@debrainwasher 🤦

    • @debrainwasher
      @debrainwasher 21 годину тому +1

      @@Paonporteur Bien sûr. C'est suffisant.

  • @Macedonia2404
    @Macedonia2404 2 дні тому

    Which chemicals are emitting radiation.and 2.4 volts Torchlight bulb diffuse

  • @thes4543
    @thes4543 2 дні тому

    Why won't you make a video about NITRONIUM perchlorate?

    • @ChemicalForce
      @ChemicalForce  День тому

      This is a very complex synthesis and the precursors are not easy to synthesize. First we need to work out the method of obtaining N2O5

  • @alcidecloridrix9309
    @alcidecloridrix9309 2 дні тому

    If I had been showed the structure of this compound without knowing it existed in real life...
    "Hmmm, the bonding looks right, but ... il looks kinda sus....."

  • @jaimeortega4940
    @jaimeortega4940 2 дні тому

    The explosion was combustion just spread out with ethanol.

  • @gv100_blitz
    @gv100_blitz 2 дні тому +3

    Why does bro have phenyl hydrazine??? We may never know😂😂😂😂

    • @hantrio4327
      @hantrio4327 День тому

      He has everything

    • @MrYellowOffical
      @MrYellowOffical День тому

      It’s a pretty normal chem for some things I also made it in a video lol

    • @MrYellowOffical
      @MrYellowOffical День тому

      He has some pretty exotic chems though

  • @gv100_blitz
    @gv100_blitz 2 дні тому

    These reactions look a lot like solid rocket fuel burning lol

  • @guythat779
    @guythat779 2 дні тому

    Bro casually has a boran complex

  • @JoakimfromAnka
    @JoakimfromAnka День тому

    "Commercially avaialble perchloric acid" almost sounds like you could walk into a hardware store and buy it.

  • @lotharmayring6063
    @lotharmayring6063 День тому

    i do not like to work with this explosive substanzes and i do not think that it make much sense to burn them

  • @xfxox
    @xfxox День тому +1

    Pretty evil substance

  • @dennisford2000
    @dennisford2000 День тому

    Burns like a small star and collapses into a black hole

  • @МельникВладимир-я2ц

    May be velocity of detonation with you

  • @MadScientist267
    @MadScientist267 День тому

    So basically what you're saying is... OXIDIZE!! 🤣

  • @MaxCarponera
    @MaxCarponera 2 дні тому

    "Close to 70%" - NOT NICE

  • @МельникВладимир-я2ц

    Thank you
    I love your channel🎉❤😊

  • @МельникВладимир-я2ц

    Dekaborane with noclo4😂?