The Fourier Transform in FTIR Spectroscopy

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  • Опубліковано 4 січ 2025

КОМЕНТАРІ • 40

  • @jesusm1583
    @jesusm1583 6 років тому +28

    I´a m chemical engineer and I can say that the content of this video resumes almost 3 university courses or more depending the schoool, amazing how much talent is here!

  • @eoliveira2711
    @eoliveira2711 2 роки тому +4

    One of the best presentations of Fourier transform applied to spectroscopy. Not only that, but apodization, resolution, etc. Thank you for making this so well!!

    • @hetong7814
      @hetong7814 Рік тому

      Do you know why FTIR need interferometer?

  • @baha3043
    @baha3043 Місяць тому

    Thank you! It really helped me prepare for my presentation. The quality of the presentation is outstanding!

  • @jennysilvestre123
    @jennysilvestre123 4 роки тому +1

    Your video really helps me a lot! Fourier transform is a bunch of integration and I don't understand it just by reading journal articles. You made it easy and simple! Thank you!

    • @barrylinkletter
      @barrylinkletter 4 роки тому

      Thanks for your comment. I should emphasize that treating it as a series of integrated cross products (multiplication) of sample signals and test frequencies is a simple way to explore the idea but the actual math is much more powerful. I don't have a clue how to do real math so I stick with calculus. I am glad that my interpretation was helpful.

  • @DrMrmld
    @DrMrmld Рік тому

    Really enjoyed this presentation. Many thanks for your work, I greatly appreciate it!

  • @mrbbizzle
    @mrbbizzle 4 роки тому +2

    I wish I could give you a high five and buy you a beer for these incredible lectures!

  • @sujiang7256
    @sujiang7256 3 роки тому

    The best presentation I've ever seen!

  • @sudhakarg2012
    @sudhakarg2012 6 років тому +4

    Fantastic lecture on UV/vis and IR spectroscopy! Would love to donate to your channel.

  • @malonelee1001
    @malonelee1001 5 років тому +3

    Lovely, should have been on youtube back when I was studying!

  • @paulam.1268
    @paulam.1268 2 роки тому

    taking the red pill is never easy but I loved the lecture! Thanks so much! :)

  • @ismailsarwar733
    @ismailsarwar733 4 роки тому

    After taking the lecture from the Prof. Linkletter, I really want to go to his university and take lectures from him.

  • @黃少柟
    @黃少柟 5 років тому +1

    Best explanation I have ever seen

  • @РусланДементьев-с7п

    Thank you very much!! Very clear ans concise explanation of the content🔝

  • @hw093
    @hw093 4 роки тому +2

    finally I understand fourier transformation!! 😍

  • @sammystuhlman2191
    @sammystuhlman2191 5 років тому +4

    I dont know exactly what is going on, but some of the early math is wrong (or stated incorrectly). for example the integral of cos(5x)*cos(5x) from -.5 to .5 does not equal 1, in fact cos(whatever)^2 is equal to 1 - sin(whatever)^2 so it is always less than one. It is still a really good explanation wise, but something is wrong with the early math (around 2:40).

    • @nvd-1325
      @nvd-1325 Рік тому

      that is integartion with span=1 ( the area)

  • @himaghnabhattacharjee4654
    @himaghnabhattacharjee4654 3 роки тому

    This is lovely. Thank you so much

  • @prunoivo7045
    @prunoivo7045 5 років тому +3

    That is amazing lecture. Thank you so much ! I have a question. What can the intensity of FTIR peaks tell us about ? What is the meaning of the intesity in FTIR ?

    • @keynotechem
      @keynotechem  5 років тому +2

      The ratio of observed intensity to original intensity of IR light is what is reported in a typical IR spectrum output. If a peak is at 20% intensity that means that 80% of the IR light was observed at that wavelength. By converting the ration to absorbance we can obtain a number that is directly proportional to concentration. Abs = -log[I(out)/I(in)]. If we know the molar absorptivity for a given substance at a given wavelength we could use the abs value to calculate concentration. This would only work where we have a dilute solution (usually in chloroform). Other IR methods using thin films or KBr pellets to mount the sample would not give results where concentration has much meaning.

    • @prunoivo7045
      @prunoivo7045 5 років тому

      @@keynotechem Thank you very much for your answer !

  • @hetong7814
    @hetong7814 Рік тому

    One of the best presentations of FT, but i still din't understand why need to use interferometer, can we just use different frequencies of light are shone on the sample simultaneously then do FT? why need interferometer.

  • @jose_475
    @jose_475 Рік тому

    This is AMAZING

  • @navminaik1626
    @navminaik1626 5 років тому

    Awesome video. Thank you so much!!

  • @Pornchairakpongsiri
    @Pornchairakpongsiri 3 роки тому

    For FTIR instrument, the IR source come with single or multi wave length?

  • @Pornchairakpongsiri
    @Pornchairakpongsiri 3 роки тому

    Great vdo!

  • @josuemena16
    @josuemena16 4 роки тому +1

    but, how can we get a function of the FTIR interferogram that we can put into the Fourier transformation?

    • @barrylinkletter
      @barrylinkletter 4 роки тому +1

      That is where real mathematics comes in. I used a continuous function made up of a set of combined cosine waves and tested it with a single cosine wave of a chosen frequency. The integration of the product will give an answer of 1 if the frequency is present and zero otherwise. However you will see in the presentation that there are serious limitations to this approach and it is not a "real world" application. In the FTIR, the spectrum received is a series of data points taken at set distance intervals (a multiple of the wavelength of the laser you see passing through the sample chamber). So you have a list of power received at each distance and need to turn that into a list wavelengths in the signal and their power. This is where the "Fast Fourier transform" (FFT) algorithm is used. It is designed for manipulating data points, not continuous functions. I sadly can tell you little about it, but it is famous in math and computer science and there are many videos dedicated just to the FFT available out there. My method demonstrates the idea of the Fourier transform but is useless otherwise.

  • @syedmujeebuddin7806
    @syedmujeebuddin7806 4 місяці тому

    Thank you

  • @MrPimmetjepom
    @MrPimmetjepom 4 роки тому +1

    hey! Super nice video. Could I ask you how do you make these kind of presentations, like what program?

    • @keynotechem
      @keynotechem  4 роки тому

      I made the slides in Adobe Illustrator and then copied them over to Apple Keynote to set up the slides. All the transitions are "magic move" transitions where I copy the slide, change elements and the transition takes care of any movement, scaling or fading/appearing.

    • @MrPimmetjepom
      @MrPimmetjepom 4 роки тому

      @@keynotechem thank you, it looks very nice

  • @gustavobolanos8109
    @gustavobolanos8109 4 роки тому

    Excellent!

  • @ivanantonov4889
    @ivanantonov4889 9 місяців тому

    Great!

  • @raymondzhao9557
    @raymondzhao9557 3 роки тому

    very interesting

  • @pharmasolutionpakistan7668
    @pharmasolutionpakistan7668 3 роки тому

    Good

  • @x00g40
    @x00g40 5 років тому +2

    you are Jesus

  • @hetong7814
    @hetong7814 Рік тому

    One of the best presentations of FT, but i still din't understand why need to use interferometer, can we just use different frequencies of light are shone on the sample simultaneously then do FT? why need interferometer.

    • @keynotechem
      @keynotechem  Рік тому

      That could be done. However then you need either a diode array detector or the machinery to move a diffraction grating so that the light crosses a detector as the grating moves. In that case you would not need FT as you are analyzing the energy at each discrete wavelength. UV-vis spectrophotometers use this method.
      IR wavelengths make the use of the interferometer convenient and less expensive than continuous wave systems (like UV-vis). Diffraction gratings for IR are difficult to make but not impossible. I myself am not familiar with all the limitations and advantages of both approaches but clearly for IR the industry has chosen interferometry for its effectiveness, cost and convenience in this wavelength range.