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Hydrogen, Time
Приєднався 2 лют 2019
A channel with science and engineering content. Mostly chemistry and electronics.
Reverse engineering and modulating ebay laser diodes
In this video I reverse engineer the circuit that drives cheap 5mW laser diodes, find a few surprises, modify the circuit and try to modulate the laser output with digital data.
Переглядів: 1 476
Відео
Simplest loudspeaker oscillator
Переглядів 2,6 тис.8 місяців тому
An even simpler audio oscillator than the one featured in this article: hackaday.com/2024/04/23/no-active-components-in-this-mysterious-audio-oscillator/ Although I assume somebody else surely came up with this design before, I independently invented this speaker oscillator when I was a kid, by trying to wire a speaker to an already connected battery, hearing it making noise and figuring out why.
First neon tube
Переглядів 244Рік тому
Testing of my vacuum manifold by making my first neon tube. Use of magnesium as getter to make neon tubes reference: hackaday.com/2023/04/20/making-neon-trees-the-easy-way-with-no-oven-pumps-required/
Does my lamp prototype produce X-rays?
Переглядів 294Рік тому
First glassblowing experiments to make fluorescent tubes.
Electronic ballast repair
Переглядів 904Рік тому
Reverse engineer and fix of an electronic ballast for fluorescent tubes.
Titanium chemistry - Make metatitanic acid
Переглядів 5272 роки тому
References: ethesis.nitrkl.ac.in/5383/1/109CR0551.pdf thesis "Preparation and Characterization of Barium Strontium Titanate Ceramics by Gel-Combustion Technique." p21 Titanoxy sulfate intermediate book "Handbook of preparative inorganic chemistry" G. Brauer p1228
Process 01: An open source 2 layer PCB process - part 2
Переглядів 9 тис.3 роки тому
This video presents Process 01, an open source 2 layer PCB production process, including electroless copper plating of vias. In this second part I will detail the preparation of all chemical solutions required by the process. hackaday.io/project/180422-process-01-an-open-source-2-layer-pcb-process Resources referenced in the video: The plating baths shown in this video are an adaptation of form...
Process 01: An open source 2 layer PCB process - part 1
Переглядів 31 тис.3 роки тому
This video presents Process 01, an open source 2 layer PCB production process, including electroless copper plating of vias. In this first part I will go through all the 31 steps required to make a double sided printed circuit board, while in the next video I will detail the preparation of all chemical solutions required by the process. hackaday.io/project/180422-process-01-an-open-source-2-lay...
Make P22B a blue phosphorescent material
Переглядів 1,1 тис.3 роки тому
How to make ZnS:Ag or P22B, a phosphorescent material used in cathode ray tubes (CRTs). Links: Inorganic phosphors book: www.sciencemadness.org/whisper/files.php?pid=654604&aid=86683 Standardized phosphor table: bunkerofdoom.com/tubes/crt/crt_phosphor_research.pdf Willemite synthesis: ua-cam.com/video/_qg6AnqgxDA/v-deo.html Sulfur purification: ua-cam.com/video/Ki3NC0kjWQ8/v-deo.html Silver nit...
Make pure Silver with Vitamin C
Переглядів 7683 роки тому
In this video I'll purify silver nitrate. In one step, we need to reduce the resulting silver oxide to silver metal powder, and to perform this operation, I'll use Vitamin C as a reducing agent.
Hot ice
Переглядів 1233 роки тому
How to make hot ice at home with sodium acetate and water. The recipe is to add 7.4 ml of water for every 10 grams of sodium acetate. Technology connections video: ua-cam.com/video/Oj0plwm_NMs/v-deo.html
Towards an open source 2 layer PCB process
Переглядів 9153 роки тому
Some progress in making double sided PCBs. Image of PCB factory in the video taken form Wikipedia (en.wikipedia.org/wiki/File:PCBs_hanging_in_electroplating_machine.jpg)
Make pure sulfur crystals
Переглядів 6 тис.4 роки тому
How to increase sulfur purity by recrystallization from xylene.
Chlorobenzene from NaDCC
Переглядів 8914 роки тому
Synthesis of chlorobenzene using Sodium dichloroiscyanurate (NaDCC).
The tetranuclear copper(I)-pyridine-iodide cluster
Переглядів 7554 роки тому
Tetranuclear copper(I)-pyridine-iodide cluster references: woelen.homescience.net/science/chem/exps/fluorescent_copper/index.html pubs.acs.org/doi/abs/10.1021/ed200736b Pyridine synthesis videos: NileRed: ua-cam.com/video/r-xt24lBbrs/v-deo.html Doug's Lab: ua-cam.com/video/FNsqYwzm40M/v-deo.html Extractions&Ire: ua-cam.com/video/3KrjbIp-Za0/v-deo.html N2H4 Labs: ua-cam.com/video/V2SI0f3n9u4/v-d...
100 subs, NileRed citation, phosphors and more
Переглядів 5754 роки тому
100 subs, NileRed citation, phosphors and more
Make high quality PCBs at home: an overview
Переглядів 6875 років тому
Make high quality PCBs at home: an overview
Oscilloscope repair: Unaohm G421E DT
Переглядів 1,1 тис.5 років тому
Oscilloscope repair: Unaohm G421E DT
Making ZnS:Cu, a green phosphorescent material
Переглядів 22 тис.5 років тому
Making ZnS:Cu, a green phosphorescent material
👍👍👍
Really nice video, thanks for sharing. One Question though, how do you avoid solder mask from going inside the holes when applying it in the end? in my case it got stuck in some holes and even though it wasn't cured because of mask blocking the pads, it didnt dissolve by itself and i had to use a drill bit to poke it out. probably cause i had too small holes for this?
Well explained about the PCB process.
Thanks for the video! Very Good and Learned something new today!
Case is connected to the positive terminal because of what these lasers are mostly used for. They are mostly used for laser pointers and these are usually powered with coin cells. Coin cells have positive electrode on the outside. Thanks to that, positive of the diode and positive of the cell can be connected with metal case of the pointer, making the device simpler and cheaper. Cheapest modules have a simple resistor instead of the regulator.
Great info, thanks! I didn't know what was in these cheap devices, so I bought a few individual laser diode components. They have the built-in photodiode for monitoring output, but I wanted to try using it for self-interferometry measurements. One laser diode has that weird arrangement with the case as common anode, so I don't know how to work with that. My other is common cathode :) But I realised I needed a heatsink & optics to focus the beam, so bought a cheap case+lens kit. Now I need a small vice to press the diode into the fitting :( And for some reason each of these parts are more expensive than a pack of the cheap modules you're using :(
I attempted this via the I2C bus from an ESP32 to modulate the diode. I then added 10 diodes on the subsequent additional multiplexes to light up an oak tree for Christmas in the wood behind us. All rather pointless but fun nonetheless!
will this flash brighter under intense impact?
Awesome !
It works, but I have to prepare electroless copper solution each time. In your guide you say that I need to acidify it after use with H2SO4 and make it basic using NaOH when taken out of storage before next use. Can you provide exact pH values?
pH is likely not the best way to precisely characterize the electroless solution, as I add a NaOH solution till the pH is about as basic as the NaOH solution I'm adding (don't have a pH meter, I'm using pH paper). You should basically just add NaOH solution till it's strongly basic. To characterize precisely the concentration, titration would be better, I guess.
Would you consider making a video on the synthesis of electroluminescent phosphor? It is a very cool technology.
Years ago I tried, and failed. Maybe I'll try again someday.
you are smart man, great work..
That's how a car horn works.
Niceeeeeeee🔥
great hack. thanks for sharing!
Its even tuneable if you add some mass to the cone.
If you're curious what does the waveform looks like I measured it with an oscilloscope ua-cam.com/users/postUgkx-uD0CHLhRvanLAB8pf57c0F2gAFuoBfC
I was half expecting you to reveal a small relay behind the speaker cone when you turned it over. (Relays by themselves can be wired as buzzers, of course.) I don't know if a relay counts as an active device.
In a way it is a relay, its just sharing the coil and part of the contact with the speaker.
Is this palladium based activator solution and electroless copper bath stable and can be used for months? If not then how manufacturing factories use this solution for long time?
If you keep it in a well sealed container the activator is stable for years. When the activator goes bad it also changes color becoming transparent, so it's easy to know if it's still good.
From Iraq 🇮🇶
Nice experiment. I had the idea to put lithium in a tube, seal it and create a low pressure discharge tube without a vacuum pump. Only argon, hydrogen and ammonia(from lithium nitride reacting with water vapor) should be left.
At high temperatures lithium may react with the glass though, not sure.
Your process is very expensive because you use pdcl2. I have another solution to use AgCl for activator.
Can you share it please?
Post a link to your procedure? I'm curious.
hello, please share some details
AgCl? no way, it decomposes on expose to daylight, I know how to use other silver compounds for electroless deposition, but AgCl is definitely not the way to go, for anyone wondering
@@taster2365yes with silver. activation is done in the same way as in the pictures, only a slightly different composition but the conditions are the same :) the pcb board becomes dark from the silver. then we clean it and the rest remains in the holes. anyway it works. as for the formula, I do not give it.. but there are many similar ones on google patents
please tell me is the palladium activator solution colloidal or a well mixed solution?? yours looks well mixed but I have tried it is always colloidal.....kindly clarify
I'm not sure. The dark color could be a fine suspension of metallic palladium but I did not investigate.
Nice tube! I did something very similar using titanium wire to act as both a feedthrough and to capture residual gas by sputtering. Titanium happens to be pretty well matched to soft glass when it comes to expansion, making it pretty simple to create good seals. www.dropbox.com/scl/fi/zq9pqlwfj9c97pr1ohukd/2021-10-08-23.14.52.jpg?rlkey=g6nkuw43651zwmnu1annhoaau&dl=0
Very cool. I didn't know you could use magnesium as a getter so easily, good to know!
Neat....cheers !
The yellowish collor of the Paladium Solution is because the chemicals in the solution are reducing and they need to be completed again to original levels.. normally adding some more Palladium regularly... there are some lab tests to detect what needs to be added to solutions be its a little complex to explain here...
incredible process, im really frustrated with my boards not having hole plating. thanks so much for this!
Be careful if you try to replicate this, you need to have some chemistry experience and a fumehood
@@hydrogentime2872Hello, how long do we keep it in each one?
I miss chemplayer background song ❤
Acido ascorbico , precipita la plata?.
for electro plating use a coffee filter and wrap the anodes in it to catch the large chunks of copper (do not wrap the PCB) i myself use a laser to etch double sided pcbs , i use flatcam and Lightburn to generate the cnc job , i then take a cheap pcb with copper already in it , coat it in spray paint ,and then burn the negative of the traces of the pcb on both sides with the laser , then i etch it ,and give it a green coat of paint like a solder mask , and then burn away the green paint to reveal the solder pads . its less involved since im bad with chemicals ,my reason for doing this is that shipping from pcb way or any other company is 25 $ plus so i just do it at home
Turned out the main issue was the excessive resistance of my alligator clips resulting in the two copper electrodes having appreciably different potential and trying to electroplate between them.
Graphite spray ,scrap and Sand,electrocopper,Holes are metalised...tyour laser Paint système I use too,but m'y lasers ends After a total of some hours of engraving...and i dont know why....maybe IS thé common supply of the laser with Steppers 12 v...some surges maybe during motions
Hello, Are there any substitutes for PdCl2? I can't find it at an affordable price where I live. (the only seller charges an arm and a leg for a gram of it)
There is no substitute that I know of for this process, but search on youtube for other processes. Some had success spraying conductive carbon paint and then electroplating onto that.
@@hydrogentime2872 I pulled the trigger and bought everything for this process. (Except the PdCl2, of course). I'm trying to find another supplier for it, fingers crossed. I'll post results when I actually get to do it on a real job.
An it would have been Educating if we told an shown what was the liquid in the little Amber bottle that you mixed with the Sulfur. You turned the bottle around so the label was hidden. I couldn't understand most what you were speaking. 😢
The solvent is xylene. It is also written in the initial safety notice.
do i need both electroless and electrolythic copper plating for connecting vias or can i just use one of them
You can in theory use only electroless, but it is slow to build up the desired copper thickness, and you need to fine tune the process for the surface finish to withstand the etching. Only electrolytic does not work as copper only plates to already conductive surfaces, and the holes are not conductive initially.
... Love to see more ideas with glass
The Paladium Activator sometimes turns to a yellowish transparent collor... this case You just put it inside a glass flask and this flask inside another conteiner (or a Pan for example) with boiling water for some 20 minutes, 30 minutes until the solutions turns to dark brown collor... I have made it to a lot of solutions of Paladium and it worked very well..
Will try next time it happens
Bello! Non vedo l'ora di vedere il tubo riempito di Neon. A che tensione lavora l'alimentatore?
Open circuit it overflows my oscilloscope, and the frequency is too high for a multimeter. I need a 100x probe...
Do you know why the lamp makes these discrete lines? That increase in number as the pressure increases, and have this "stepping" behavior (appearing or disappearing 1 line at a time) ?
The phenomenon is called plasma striations or plasma stratification. It's quite complex. When we are in a DC discharge, a bright anode column is formed at a certain pressure spaced out by a dark area. At lower pressure ranges, the positive column is composed of striations, or ionization waves, caused by the electrons finally having enough energy to ionize the gas, then losing the energy by ionizing it, then reaccelerating back to high enough to repeat. This causes a series of barrages of photons being released in waves, seen as striations in the plasma. In AC the anodic column moves continuously and makes the phenomenon even more complex and susceptible to other stimuli such as capacitive coupling, any resonances between the frequency and the ionized gas, etc.
Also known as 'Faraday or Crookes' Dark Space and is as you say, very complex.@@AlbertoMelappioni
Learned something new. Thanks.
You are ever one step forward but you should make videos more frequently.
Subtitle nobtranslate sir😢
sir thank you so much for making this love you so much plz one question Sir i made zinc sulphide with NA2S+ZNSO4= NASO4+ZNS CAN I USE IT TO MAKE GLOWING POWDER PLZ TELL SIR
Never tried this reaction. Assuming it does indeed make ZnS, you'll need to filter and dry the ZnS, and then proceed as in my video adding the desired dopant such as CuSO4 and fire it in a quartz tube furnace for it to glow.
Bel Canale! Continually cosi!!!
👏
based
Why is a quartz tube required to dope the zinc sulfide?
All other types of glass, including borosilicate, will melt way before the desired temperature is reached.
Nice Video, thank you very much! After many years of using "Toner Transfer" to make my pcb i now bought a UV DTG Printer and directly print the mask for the design on the board. After etching i print the "soldermask" to the pcb too. The only thing i need to get done now are the vias. Your solution looks perfect but i'm a bit worried about the Formaldehyde. I'm not a chemist, is it possible to replace it with a less toxic ingredient? Triton-X100 is even a problem in the EU, it is banned by REACH since 2021. Is there an alternative available?
The Triron-X100 could probably be replaced by another surfactant if you can't find it, but some experimentation may be required. Formaldehyde is very hard to replace, there are alternatives which are known to reduce copper salts to the metal in a controlled way but are just as toxic. If you have no chemical experience I suggest to either wait for someone to develop a safer process (NurdRage was trying for example), or to learn chemistry one step at a time before messing with formaldehyde. And build a fumehood.
did you test your vias with current? i found it very useful to do this test in the developement of my process my 0,3mm vias usually can take about 5A, 1,2mm vias could conduct even more then 25A of current with a test batch and the vias fusing at about much lower currents, i found it useful to use that as an indicator also it turns out: you can fairly use a lot of other colloid solutions for activation (even copper in NaBH4 itself), it requires an additional etching and desmearing step+ sensitation steps tho
Interesting suggestions, I did not test the vias to failure with current, but I made a few boards since I shared the process and all of them are still working fine. My smallest vias are 0.5mm. I'd be interested if you shared (maybe in a video?) your NaBH4 activation process, I don't have that chemical in my lab, but if it turns out to be useful I may try to get some.
Thanks for the detailed video, we are making this today in my physics university class. Please could you let us know if there is a way to make the ZnS:Cu into a paste/liquid to make it stick to the bottom of a glass conical flask to form a phosphorescent screen (without dripping down the sides if it is moved around). We are making a DIY cathode ray tube :)
Chapter 5 of the book Inorganic Phosphors lists some methods. You can find the book in this thread www.sciencemadness.org/whisper/viewthread.php?tid=142184&page=2
@@hydrogentime2872 Thank you !
@@hydrogentime2872 sir thank you so much for making this love you so much plz one question Sir i made zinc sulphide with NA2S+ZNSO4= NASO4+ZNS CAN I USE IT TO MAKE GLOWING POWDER PLZ TELL SIR
@@Nothingop122 assuming you made zinc sulfide, yes, you can make glow powder if you follow the process described in the video. You will need to add a tiny amount of copper sulfate and ammonium chloride, and heat the powder in a furnace.
Can this process work with electroless nickel solution?
I'm not sure traditional copper etchants can etch nickel too, if they don't you'll have problems at the final etch stage. I know nickel plating is used after copper plating when PCB gold plating is needed, as gold plating directly over copper is troublesome, but I think this is done after etching? Not sure, if I ever try gold plating I'll give more thoughts to the application of nickel chemistry to PCB manufacturing and maybe make a video. No plans yet, though.
very well describe.. thanks a lot sir.