@@taylorbarnes8373 If he's anything like Alexander Shulgin or Albert Hoffman it might have been the acid. Why did all the coolest chemists have to die.
I love this video thank you. I had the same situation of having cloudiness after NaOH was added. I asked my professor that if I should add more water to make the phases clear. He questioned why do you add water? and told me to add MTBE. But my carboxylic acid IR came out having no carboxylic peak.
Who needs PPE? It's just a little bit of strong acid and base. If you get some of one on you, just pour some of the other one on it and you're all set.
cpalacios07 yea its never a concern until you mess up making that NaOH aqueous solution and splatter solution on your face and eyes.. have fun with those chemical burns
Yes, to show how to take them apart if you have two chemicals mixed together. Sometimes you start with that mixture and need to seperate using acid/base extraction technique.
Salvia is a straight solvent extraction and the solvent is evaporated off while other Salvia leaves absorb the isolated molecule. It may seem the same in principle ;but Salvia concentrates aren't gotten by any sort of Acid/Base extraction it's achieved through solvent pulls only, the solvent pulls the molecule/alkaloid then the solvent gets evaporated and the molecules recaptured in highly concentrated amounts back into plant material ;but not the same plant material the extractions are done from, nor do you recapture the solvent making Salvia Concentrates (I'm sure there is a separation technique to actually isolate the molecule from the solvent ;but just letting it evaporate while using the plant itself to capture the good stuff works fine). What he did is very very different and actually a process of chemistry, he didn't just do a solvent pull- he used Acid/Base and solvent, with solvent only serving the purpose of recapturing one molecule while the water solubility he created by converting the Benzo was done to isolate the now water soluble molecule so that only one would remain in the solvent layer and rather than require evaporation of solvent it just required filtering and washing with water (I would bet Salvia even concentrated is a water soluble molecule that if rinsed with water would remove everything you just worked to collect). I'm not trying to be an Ahole or argumentative and only took the time to break it down for you in hopes of clearing up the misconception for you, you seem pretty passionate about the spirit plants so I wanted to share my perspective.
@@RobotronSagedon't do it! When I was a teen I ripped a bong of 100x salvia. So salvia, with salvia extract x100 on it(maybe a negligible amount less of you want to nitpick idk the companies manufacturing process.) Total out of body experience....and I have only had those.....once....twice....four times tops in life.
a lot of people with consider their glasses protective. his are quite large (maybe intentionally). it would be very awkward to put googles over those glasses.
He's only using like 10-20ml of Ether the fumes are not concentrated enough in that amount to pose a threat , he wasn't wearing gloves either and I'm sure it is for the same reason. For all we know there may have been a flow hood or something capturing the fumes as well, he didn't really break down his setup or lab environment.
+bubba1119054 he did it to strip away any impurities that were soluble in the washing solvent - it is just one of the steps to cleaning your substance. As the benzoic acid is not soluble there should be no loss of yield of the desired product (benzo) just less nasties getting left behind.
maybe you could have talked more about what is happening at each step at a molecular level rather than why you have chosen a particular size ring to sit your seperating funnel in, and why the solution is yellow. Nice experiment demonstration though.
i see that there was a thread about DMT and it somehow had a bunch of it’s comments dissociated from it. i see many impassioned and even angry dmt comments that are just sitting aloof, unrelated to any thread. kinda funny, esp since this video is only liminally related to the almost entirely different thing that is A/B dmt ext.
Elijah Ragland you're wrong. The acid base extract can be used for all kinds of things, for instance.... extraction of crystalline mescaline from san pedro cactus.
so it's people just seeing a thing for only how it directly relates to them. When people hear distilling they think only about alcohol and getting drunk. they are not thinking about all the other uses of distilling. yes you can use distilling to get drunk, you can also use it to make too many things to list. logic, math, physics, and chemistry are the practical functioning workings of reality, it's always useful to know them. Many people regard them as normally boring to learn. So if the idea of using them to help get drunk makes you excited about learning them. then it's a really good thing right?
Most of grunt work of chemistry is purifying mixtures and chemicals. so say you have a reaction that makes two chemicals. chem X and chem Y. now let's say X has a boiling point of 50C and Y has a boiling point of 50C you can not separate them by distilling you have to do something else. so this is a method is a tool for the chemistry worker that might work for separating X and Y. a lot chemistry is using best tool for the job, and knowing what that tool is by knowing the tool not memorizing instructions. chemistry is the same chemistry aliens use in another galaxy, so don't limit your self by Needing what the instructions call for understand the principles that are going on, and think about how could be improved. What is the purpose of formula for the area of a circle? could you use it to build a gazebo is that it's purpose yes, could you use it to build a telescope is that it's purpose yes, it's purpose is infinite. the area of a circle is one small part of math? this one small part of chemistry. like math, and physics it is glorious.
Can you also include a tutorial on extracting DMT from the arundo donax plant, please Because there is only one plant in my area that I could find that has DMT, thats arundo donax please help me.
Dude.... Google + forums + your brain exist for a reason. Read a damn book or something. 😂 Jesus Christ, begging a chemistry teacher for DMT extraction techniques in a global forum. What are you? The fuzz?
many teachers are people that majored in education not the subject they are teaching. while this makes them personable and most importantly "get the job" some of the more in-depth aspects of a subject they lack fundamental understanding. any subject is so vast that it's really easy to find a small area to research, that you can quickly surpass your teachers understanding. when you start to interrogate them about it publicly in front of many parents you will look gifted. the best option for them is to admit they don't know, but few are secure enough to do this they will feel they are lousing authority and overact making them look like tyrant. if done right you can get them fired and look like a gifted victim. wreck authority that can't admit it doesn't know all.
this dudes the truth. no gloves, no safety glasses, just pure hoss.
HE DIDN'T EVEN MEASURE HIS COMPOUNDS TO CALCULATE PERCENT YIELD. THE MADMAN
boxerpop82 it was the ether XD
lol
@@taylorbarnes8373 If he's anything like Alexander Shulgin or Albert Hoffman it might have been the acid. Why did all the coolest chemists have to die.
😂
@@mattw3340 Hofmann* lmao I'm being a grammar Nazi on a 2 year old comment
I love how old chemist scientists don't use any safety equipment when using chemicals that could melt your face!
Its so nice to hear someone who really knows what they are talking about explain something. This was so helpful!
WHEN U GET TO A LEVEL THAT YOU DONT EVEN NEED SAFETY..
extremely helpful! I am doing this tomorrow in lab and so now I feel better prepared.
how did it turn out ? 10 years later, how was medical school ?
I love this video thank you. I had the same situation of having cloudiness after NaOH was added. I asked my professor that if I should add more water to make the phases clear. He questioned why do you add water? and told me to add MTBE. But my carboxylic acid IR came out having no carboxylic peak.
JOHN BLACK SUPER CHEMIST Holy cow - wish I could have read this. All the weird punctuation and all caps were too much...
No fucks were given during this procedure lmao
just pour some in there, some of this, and walaa
I love it lol
You would shut your mouth if you knew whats good fer ya.
One should vent even before shaking for the first time, right after turning the separatory funnel upside down, especially when using diethyl ether.
Who needs PPE? It's just a little bit of strong acid and base. If you get some of one on you, just pour some of the other one on it and you're all set.
holy shit baking soda can treat chemical burns?
@@RobotronSage When in doubt, pour baking soda on it.
~ Confucius
Excelente video. Prácticamente una clase de laboratorio completa. Felicidades.
this bad ass sais fuck saftey im going in bare
Made me lol ^_^
Me too! Lol
He raw-dogged that shit!! hehe
he is so stoned off that ether
should have put the benzoic acid in an ice bath, it would have increased percent yield by a lot.
HCl, NaOH..... come on professor, safety gloves
He's a boss; he's on another level: safety is not a concern.
cpalacios07
yea its never a concern until you mess up making that NaOH aqueous solution and splatter solution on your face and eyes.. have fun with those chemical burns
*****
Wonder what the molar concentration is.
Agree because we talk about teaching here...
It’s 1 M concentration, really not that big of a deal
thank you for teaching me how to do my lab tomorrow!
Enjoyable. But correct my high ass if I'm wrong (because I probably am) but did he not just put chemicals together just to take them apart?
Yes, to show how to take them apart if you have two chemicals mixed together. Sometimes you start with that mixture and need to seperate using acid/base extraction technique.
justin princinsky 😂😂😂😂that’s orgo for you
That's exactly what he did lmao
THANK YOU YOU SAVED MY LIFE
In case you havnt figured it out, he explained how to extract the D from say some salvia divinorum.
Salvia is a straight solvent extraction and the solvent is evaporated off while other Salvia leaves absorb the isolated molecule. It may seem the same in principle ;but Salvia concentrates aren't gotten by any sort of Acid/Base extraction it's achieved through solvent pulls only, the solvent pulls the molecule/alkaloid then the solvent gets evaporated and the molecules recaptured in highly concentrated amounts back into plant material ;but not the same plant material the extractions are done from, nor do you recapture the solvent making Salvia Concentrates (I'm sure there is a separation technique to actually isolate the molecule from the solvent ;but just letting it evaporate while using the plant itself to capture the good stuff works fine). What he did is very very different and actually a process of chemistry, he didn't just do a solvent pull- he used Acid/Base and solvent, with solvent only serving the purpose of recapturing one molecule while the water solubility he created by converting the Benzo was done to isolate the now water soluble molecule so that only one would remain in the solvent layer and rather than require evaporation of solvent it just required filtering and washing with water (I would bet Salvia even concentrated is a water soluble molecule that if rinsed with water would remove everything you just worked to collect). I'm not trying to be an Ahole or argumentative and only took the time to break it down for you in hopes of clearing up the misconception for you, you seem pretty passionate about the spirit plants so I wanted to share my perspective.
@@RoCkShaDoWWaLkEr Bro i don't think i can handle salvia atomizer carts
I'm probably gonna be stupid enough to try tho
fml
@@RobotronSagedon't do it! When I was a teen I ripped a bong of 100x salvia. So salvia, with salvia extract x100 on it(maybe a negligible amount less of you want to nitpick idk the companies manufacturing process.) Total out of body experience....and I have only had those.....once....twice....four times tops in life.
a lot of people with consider their glasses protective. his are quite large (maybe intentionally). it would be very awkward to put googles over those glasses.
shouldn't you have a fume hood on with ether?
He's only using like 10-20ml of Ether the fumes are not concentrated enough in that amount to pose a threat , he wasn't wearing gloves either and I'm sure it is for the same reason. For all we know there may have been a flow hood or something capturing the fumes as well, he didn't really break down his setup or lab environment.
people used to get high off of ether lmao
No safety goggles or gloves ?! (twitch )
wouldnt the product at the end also contain sodium chloride?
Thanks so much, very very helpful.
It worked perfectly what do you mean?
brb I'm going to study chemistry at college
fuk it im old imma raw dog it
Is this video is about synthesis of DMT, right?
excellent
what was the purpose of rinsing the benzoic acid again there at the end when you were feeding it through the filter paper?
+bubba1119054 he did it to strip away any impurities that were soluble in the washing solvent - it is just one of the steps to cleaning your substance. As the benzoic acid is not soluble there should be no loss of yield of the desired product (benzo) just less nasties getting left behind.
maybe you could have talked more about what is happening at each step at a molecular level rather than why you have chosen a particular size ring to sit your seperating funnel in, and why the solution is yellow.
Nice experiment demonstration though.
how do I guarantee that there's no Benzoic acid water leftover in separatory funnel?
put some on your tounge
Great video. Thank you....
Wheaton College Chicago. burbs??
did you see the size of his glasses ?
What else you gonna use it for wanda?
i see that there was a thread about DMT and it somehow had a bunch of it’s comments dissociated from it. i see many impassioned and even angry dmt comments that are just sitting aloof, unrelated to any thread. kinda funny, esp since this video is only liminally related to the almost entirely different thing that is A/B dmt ext.
Elijah Ragland you're wrong. The acid base extract can be used for all kinds of things, for instance.... extraction of crystalline mescaline from san pedro cactus.
so it's people just seeing a thing for only how it directly relates to them. When people hear distilling they think only about alcohol and getting drunk. they are not thinking about all the other uses of distilling. yes you can use distilling to get drunk, you can also use it to make too many things to list. logic, math, physics, and chemistry are the practical functioning workings of reality, it's always useful to know them. Many people regard them as normally boring to learn. So if the idea of using them to help get drunk makes you excited about learning them. then it's a really good thing right?
@@dexterj5615 or basifying a isomerized CBD (cbd -> delta 8 THC) solution to prepare for extraction / seperation 8^)
@@Amipotsophspond You can also use getting drunk to help with logic, math, physics, and chemistry!
@@Amipotsophspondyou know, you may have realigned my perception on this topic.....food for thought. I like constructive criticism. Thanks friend.
we need so we can enlightened enough.
You're a boss.
....and gloves!
i need dmt please help
dhampir1000 You can make by Yourself.
Thanks for this
did he ever help?
hey guys, who can help me with the amount of chemicals needed to carry out this experiment. Appreciatate it.
the zoom of the flow diagram doesn't help...
Dear friend I am looking for a way to install meth ace crystal
USE ÉTER?
What is the purpose of this?
Most of grunt work of chemistry is purifying mixtures and chemicals. so say you have a reaction that makes two chemicals. chem X and chem Y. now let's say X has a boiling point of 50C and Y has a boiling point of 50C you can not separate them by distilling you have to do something else. so this is a method is a tool for the chemistry worker that might work for separating X and Y. a lot chemistry is using best tool for the job, and knowing what that tool is by knowing the tool not memorizing instructions. chemistry is the same chemistry aliens use in another galaxy, so don't limit your self by Needing what the instructions call for understand the principles that are going on, and think about how could be improved. What is the purpose of formula for the area of a circle? could you use it to build a gazebo is that it's purpose yes, could you use it to build a telescope is that it's purpose yes, it's purpose is infinite. the area of a circle is one small part of math? this one small part of chemistry. like math, and physics it is glorious.
mature experienced guy 8)
where yo googles doc. epic fail
That funnel reminds me of the steroid making days back in the 90s
Brother of Dr. King Schultz
As do I my friend, as do I...
enlightenment has now foreigner. dmt is in the body anyway
WOW Cut at the end when it didn't work.
Can you also include a tutorial on extracting DMT from the arundo donax plant, please
Because there is only one plant in my area that I could find that has DMT, thats arundo donax please help me.
Do a food safe extraction if you're starting out
Dude.... Google + forums + your brain exist for a reason. Read a damn book or something. 😂 Jesus Christ, begging a chemistry teacher for DMT extraction techniques in a global forum. What are you? The fuzz?
Flurry known or fluorines!?
EXACTLY!!! ive been serching was that was
benzoic acid and what???
breaking bad
this is fucking hilarious
He's got big peen energy playing with that stuff like it's water
Um...why not mix them in the first place?
where are your googles sir ???
all professors look the same
I make that in a trailer lol
Can you add to much lye
what's the point of this
Because alligators don't have lips, duh
Because alligators don't have lips, duh
nice ty
Send me a PM I can tell you how.
NotPercy203 hey would you know how to extract just the codeine from the alkaloids ??
.
Walter white?
6:23 if a student doesn't know this he should better go back to elementary school.
oh don't be like that pls
Farmer PhD...
no
Our teachers does not teach anything like this
many teachers are people that majored in education not the subject they are teaching. while this makes them personable and most importantly "get the job" some of the more in-depth aspects of a subject they lack fundamental understanding. any subject is so vast that it's really easy to find a small area to research, that you can quickly surpass your teachers understanding. when you start to interrogate them about it publicly in front of many parents you will look gifted. the best option for them is to admit they don't know, but few are secure enough to do this they will feel they are lousing authority and overact making them look like tyrant. if done right you can get them fired and look like a gifted victim. wreck authority that can't admit it doesn't know all.
You don't need a foreign substance to become "enlightened."
Please explain
should have put the benzoic acid in an ice bath, it would have increased percent yield by a lot.