Platinum Refining Bromate Hydrolysis Pt6

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  • Опубліковано 4 лис 2024

КОМЕНТАРІ • 216

  • @JossWaddy
    @JossWaddy Рік тому +13

    What a great series. No need for any apology. Success isn't necessarily measured in the purity of the button that you get at the end, nor from the yield percentage from your starting material. On a channel like this, it's the informative entertainment you give us, all while showing the lessons you learn along the way. You risked exposure to some very nasty substances to demonstrate advanced skills and techniques, which showed us just what a huge challenge this particular tributary of chemistry involves. You have our deepest respect and gratitude and I have newfound appreciation for just how difficult, subtle, finickity, and frustrating platinum refining must be. Thank you very much for taking this on. 100% a successful series of videos.

  • @Halloween111
    @Halloween111 Рік тому +5

    Nothing wrong with backing up and punting. Sometimes, It is most helpful to know what you don't know and proceed accordingly. Hats off for all the work you put in. Experiments are how we learn. Therefore, there are no unsuccessful experiments, only successive learning experiences. Glad to come with you for the ride.

  • @recoilrob324
    @recoilrob324 Рік тому +11

    Wow! You worked HARD for that little button! I've learned a lot watching your video's....and this one taught me to never mess with refining platinum! Thanks!

  • @AndyGraceMedia
    @AndyGraceMedia Рік тому +30

    Great news you didn't give up on that pesky platinum! You did a good job - calcining was the best choice to get that metal back. Glad you wore a respirator and you still should have a gram or two in the waste destined for the stockpot. A very difficult job - you're a far braver man than this humble correspondent! And congrats on crossing 200,000 subs!

  • @HomeGrownMetals
    @HomeGrownMetals Рік тому +8

    wow, from all of us hobby refiners a take my hat off and thank you for the huge effort and work put into this series. Every single stage seems soooo much more difficult compared to gold and silver, bravo bravo

  • @Playrough_Havoc
    @Playrough_Havoc Рік тому +47

    No need to apologize you risked yourself for our entertainment and regardless of which process was used and we all enjoyed watching! Thank you for constantly giving us something to look forward to and keep up the great work!!
    P.S if you need to take a break please do so because your health is more important to us than anything else.

  • @davidtwining4059
    @davidtwining4059 Рік тому +1

    I'm glad you were able to conclude this little mini series on pesky Platinum. My patients were rewarded

  • @Der0Nibelung
    @Der0Nibelung Рік тому +5

    After watching your videos and learning to refine my own gold/silver, I am a firm believer that I will NOT be refining platinum. Thank you shipmate, for all that you do!

    • @matthewf1979
      @matthewf1979 Рік тому +1

      Wise decision! I would just collect the slimes in a stock pot and send them out to a refiner/buyer. The risk isn’t worth the price of the amount a hobbyist home refiner would ever deal with.

  • @tonydalton6756
    @tonydalton6756 Рік тому +2

    What a brilliant series Sreetips. You were akin to working on the space shuttle at times. There is definitely no need to apologise, not many people would have the nerve to even attempt it. Well done for your attempt.

  • @iamcarsberry3636
    @iamcarsberry3636 Рік тому +4

    You have to be one of the most persistent people in the world… your determination is through the roof ….. I watched all 6 videos to make it to this button I guess for the future you’ve learned alot I sure have… thanks

  • @hobbiesrus
    @hobbiesrus Рік тому +5

    Thanks Kevin. This was a tough series for sure. You put your health at risk for filming these videos, and I hope it was a good series to warn home refiners away from trying to tackle this. What a mess it makes during the precipitations and drying. All for 10g of Pt. Good job, and special thanks for including the mistakes, troubles, and guesses as you went.

  • @merc7105
    @merc7105 Рік тому +1

    Your perseverance is commendable. That button looks amazing. Thank you for sharing this series.

  • @baobao7671
    @baobao7671 5 місяців тому

    Such an awesome series. Compared to gold refinement, platinum refinement is MUCH harder! After watching your videos, I understand why jewelers charge a lot for manufacturing platinum jewelry

  • @Fambamm-ib6pw
    @Fambamm-ib6pw Рік тому

    No apologies needed, you furthered your knowledge and this was awesome to watch 👏

  • @newtronix
    @newtronix Рік тому

    A highly enjoyable series. Thanks for all the effort.

  • @CrimFerret
    @CrimFerret Рік тому +4

    Thanks for the series of videos. You took a lot of risks with those. You showed very well how difficult it is to refine that metal. I don't think there'd have been anything to gain by going any further. Anyone who watches this series and still thinks it's cost/risk effective to do at home simply will have to learn the hard way I guess.

  • @Jroctpl
    @Jroctpl Рік тому +1

    ST, u making me nervous moving around that lil dish. I learned (from you) that's not safe stuff to be handling. I hope u don't mess with that stuff anymore as your gold and silver videos have brought me so much knowledge and entertainment over the years. Be safe sir, can't wait for the next post

  • @ArielleViking
    @ArielleViking Рік тому

    Refining platinum is obviously a very involved and complicated process that I never realized. A very interesting series and that sure looks a pretty button. No need to apologize, it was all fascinating. 👍

  • @1911darkstar
    @1911darkstar Рік тому +2

    Fascinating series. It’s interesting how different the PG metals are to the usual Gold and Silver. As you have stated in previous comments in this series, refining gold seems almost easy compared to working with platinum. Really appreciate the fact you attempted this purely for content for the channel even though you were not sure how it would end up. Too many UA-cam producers are more concerned with a slick, prod

  • @donnakawana
    @donnakawana Рік тому

    Your amazing Sir!! What a beautiful button.. The amount of work an dangerous position you were in to do this... Grateful doesn't quite cover the thanks I give an Honor Sir StreeTips!!
    Thanks DK

  • @jonahweinshenker
    @jonahweinshenker Рік тому

    Excellent series but gold is so much more satisfying to watch and so much safer. We appreciate you.

  • @daviddpg
    @daviddpg Рік тому

    That was a ton of work. You are a more patient man than I. Nice job.

  • @KiwiKoNZ
    @KiwiKoNZ Рік тому +1

    16:47 The best part of all 6 episodes! 🔥👈🤩👍✨

  • @DJDream
    @DJDream Рік тому +3

    after watching this series... I have a few suggestions... I fell like a seperatory funnel would save you a ton of time with all the back and forth you were doing that and dish washing and solvent.. also because you are dealing with such fine particles you should really double or triple up on your filter papers or use a sintered glass funnel! =) my two cents anyways! FYI Love the content! =)

  • @asjamuir5534
    @asjamuir5534 Рік тому

    Excellent mini series on platinum 10/10 I think u said in a early episode that u need better hoods etc for platinum for it to be safer than u did in this I appreciate the attempt better than most people can do a humble man is a honest man and that is you show the process error knowledge gaps and successes

  • @wilsonrawlin8547
    @wilsonrawlin8547 Рік тому

    Still was successful for the most part! Fun watching you fight it all the way, Chief. The dangers of the fumes/inhalants was too great to keep going. Nice looking button!

  • @shaneyearby4438
    @shaneyearby4438 Рік тому +2

    Very nice button and a great series just to show how difficult platinum can be. Bravo sir 👏 can't wait to see what you have for us next.

  • @CuttinEJ
    @CuttinEJ Рік тому +6

    No apologies necessary, Chief. This was a very interesting series and a difficult process. If you ever figure out how to separate the other metals from the Platinum I’m sure I won’t be the only one who would like to see how it’s done. Good job!

  • @WaffleStaffel
    @WaffleStaffel Рік тому +3

    I use a spray bottle to knock down the stuff floating on the top. To avoid adding excessive water, I also use it to wash the sides, instead of using a wash bottle. I use one of those continuous mist spray bottles.

  • @edwardsmith9049
    @edwardsmith9049 Рік тому +1

    Thank you so very much. There was no reason to apologize. I think 🤔🤔 you did a very good job. I never knew that it is so much work. The people that makes it. Must get paid a lot of money. I always enjoy your content. You make it interesting.
    Keep up the great content. Look forward to seeing your videos.
    Sorry 😔😔😞 I can't spell. Real Talk 101 !!!!

  • @briandillon3543
    @briandillon3543 Рік тому

    No need to apologize. I think you were successful in refining the platinum. Way more successful than I could've done. Congratulations on going as far as you did.

  • @pixill4ted593
    @pixill4ted593 Рік тому

    Excellent job, I really enjoyed this series. Thank you

  • @neilroy4090
    @neilroy4090 Рік тому

    Nicely done!!!! there is always next time that the wonderful thing about this there is always time to learn and achieve.

  • @EnnPeeCee
    @EnnPeeCee Рік тому

    Your tenacity is impressive, Mr Sreetips!

  • @nathanvanlieshout7834
    @nathanvanlieshout7834 Рік тому

    Thank you Mr Sreetips for this series.

  • @larryevans7669
    @larryevans7669 Рік тому

    beautiful work. always best to stay safe. Thanks for everything.

  • @joy_is_purple
    @joy_is_purple Рік тому

    You did well. No apology necessary. Thank you for educational entertainment!

  • @titanicfilmsbymark
    @titanicfilmsbymark Рік тому

    That was a lot of work for you. Great series of videos

  • @weedwacker1716
    @weedwacker1716 Рік тому

    I'm glad you called it. I've been worried that the videos and your channel would end abruptly with no explanation.

  • @D_A86
    @D_A86 Рік тому

    Certainly one of the more tricky refinings I've watched you do. Definitely appreciate the risks you take to make these series 🫡🙏

  • @MostlyIC
    @MostlyIC Рік тому

    AOK, still very educational and entertaining with or without the bromide process,

  • @richiebthebarberbowens4193
    @richiebthebarberbowens4193 Рік тому +3

    Couldn’t wait lol. Hello my friend

  • @spamaccount6460
    @spamaccount6460 Рік тому +1

    That looked quite nice and shiny in the end. Just by looking, you'd think it was so pure!

  • @tombrooks3812
    @tombrooks3812 Рік тому

    😊Bravo, its a thing of beauty. Persistance will get you there. Thankyou that was great watching it finally melt into a little ball. Platnium sure is a good lookin metal. Stay safe and have a great day.

  • @marcyd2007
    @marcyd2007 Рік тому

    Well done Sreetips! It wasn't the test you wanted, but you still got nice little button out of it. Thanks for showing us. Now go get Mrs Sreetips a nice bottle of wine, moonshine or whatever she drinks for putting up with you and your chemistry set in the garage 🙂

  • @Knee-ko
    @Knee-ko Рік тому

    Congrats on the end result @sreetips. A little beauty which doesn't do justice to the time and risk you put into it 👍👍

  • @jewellerydesignerartists9353

    Beautiful process ❤️

  • @tomahawktom7595
    @tomahawktom7595 Рік тому

    Good job and a good series. Bet you’re happy you’re done with it

  • @dawnjennings4864
    @dawnjennings4864 Рік тому

    That’s a really good looking button! Well, done, my friend!

  • @guyhiebert
    @guyhiebert Рік тому +3

    Very interesting to watch how much you had to do to get to 9.9 grams. And of the dangers and the safety measures that you also took.

  • @matthewtracy8744
    @matthewtracy8744 Рік тому +1

    Safety first man! Great series!

  • @ruckusflow
    @ruckusflow Рік тому

    A great effort very much appreciated, thank you!

  • @thegoodlookinorange1986
    @thegoodlookinorange1986 Рік тому

    On your filter paper there was precipitate when you tested it that’s all. Always great content SREETIPS.

  • @anthonywaite
    @anthonywaite Рік тому

    Been looking forward to this video... nice work buddy thank u for showing us so we can learn with u

  • @mickg6480
    @mickg6480 Рік тому

    From the 2nd part on, it was very evident how difficult and frustrating this experiment was for you. As informative as it was, I struggled along with you. A meagre result in the end to boot. You'll get 'em next time though 😉

  • @tom23rd
    @tom23rd Рік тому +1

    Yessir, can't wait to see how this resolves! 😎🔥👊

  • @adamsaint5879
    @adamsaint5879 6 місяців тому

    HA! really enjoyed this series.. You are a trooper. Personally Id make a new lab rule. no platnum! right when you came back after trying to evaporate the milkshake fromt he fused quartz. seeing that mess... you contained what Im sure was something akin to "I hate this soup" off camera well. thanks for the attempt, very entertaining, certainly... those platnum rings, were pretty good as platnum rings ;)

  • @bengoose2031
    @bengoose2031 Рік тому +5

    The main thing I learned was every step of platinum refining is extremely difficult and dangerous.

  • @NOFX0890
    @NOFX0890 Рік тому

    Great Effort Sreetips...
    Win or lose you got a Wagyu Steak and I hope it was great.
    Thanks for sharing... it was still an interesting series.

  • @austinsinclair6827
    @austinsinclair6827 Рік тому

    Just found your channel. Love your voice, love your content, and love your dedication. Thanks for making these videos their very theruaptic!

    • @austinsinclair6827
      @austinsinclair6827 Рік тому

      And the fact that your the only UA-camr I've ever seen to like so many comments and reply is so beautiful

    • @sreetips
      @sreetips  Рік тому +1

      Welcome! And thank you

  • @Antonowskyfly
    @Antonowskyfly Рік тому

    You’re welcome. It’s a well produced series with a substantial effort put in to the topic/subject and surely your call to err on the side of caution is .99999fine correct. The resulting button may just about cover the next family get together at the steakhouse! Thank you Sir! 👍👍🤟

  • @patrickaussieMilartry
    @patrickaussieMilartry Рік тому

    Always loved the casserole dishes I'm not 100% but they look like 1970+ Pyrex or fire glass. ANYHOW they are cool to collect. Sorry to go off track their but they are great tuff old wearing dishes. 👍

  • @bfd1565
    @bfd1565 Рік тому

    Oh boy, this was a tough one. I bet you're glad this video series is over. Interesting stuff Sreetips.

  • @ColonelH
    @ColonelH Рік тому +1

    Great series Sreetips. Not as satisfying as Gold but an extremely interesting process for sure. Be well!

  • @philbartoli2011
    @philbartoli2011 Рік тому

    Nice work congrats on 200k 🎉🎉

  • @Mike-ou5ps
    @Mike-ou5ps Рік тому

    Howdy Sir...
    FINALLY got that sucker done, lol. That's insane how much time and effort it takes to make that platinum. Note to self, "Don't mess with Platinum".
    All that time for a $400 button, WOW man, that's dedication Sir. I made more delivering pizzas back in the day in much less time. I'll never look at a Platinum ring the same again.
    With the effort it takes to refine Platinum, you'd think it'd be worth more than $34.31 a gram.
    Respect to your effort 👌. I spend weeks doing detailed wood carving and started watching your videos cause I want to start adding gold inlays to my carvings and jewelry boxes.
    Craftsmanship is an acquired skill. I'm starting to wonder if I'm underpricing my skill. Hmmmm.

  • @arnedalbakk6315
    @arnedalbakk6315 Рік тому

    Hello Mr sreetips. It is so cool whit the timelaps. This must be on of your tuffest task sir. Great clip. Arne

  • @timsmith9645
    @timsmith9645 Рік тому

    Nice platinum button sreetips thanks for sharing

  • @aussienscale
    @aussienscale Рік тому

    Awesome effort mate, very much enjoy the videos, no need to apologise at all !

  • @tonyc3858
    @tonyc3858 Рік тому +1

    Good Lord, the precipitation process makes a forbidden milkshake...

  • @Etoxiran
    @Etoxiran Рік тому

    Hi Kevin, great video - no need to apologize. It is not fail, a lot can be learn from this series. Processing PGM is hard to do in backyard, I regret to wait for salary next week and can't bid on this one shiny button. Pt salts are nasty to work, and this method still be mysterious until reinvented [or somebody who know, will share his approach]. I learned about this procedure [not sure if this is from C.M. Hoke?] some time ago, looked for Pourbaix diagrams and tried to found more information- it's easier to find nuclear fuel reprocessing that this reaction 🙂
    These salts should be kept away from spattering as much as possible. Filtering on paper placed over sintered glass filter [cleaning this is worst part] from excess of liquid before heating would be more efficient for work with this & quartz dish.
    Refiners use quartz tube with furnace on them/heating element - with dried salt inside for calcination [and salmiac collecting in another container] and better temperature control. I met same problem with these salts - it's easy overheat them. Building simplest appropriate setup would cost similar to value of your metal itself [temperature can be regulated manually, but it would better to use PLC & thermocouple to run it slow instead babysitting this all day].
    PS. Did you measured button density??

    • @sreetips
      @sreetips  Рік тому

      No density. Platinum refining is far above me. But I learned much

  • @Heymrk
    @Heymrk Рік тому

    A good senior chief always gets the job done. It may not have been perfect, but you were an NCO-- you work for a living.

  • @cziprick
    @cziprick Рік тому +1

    That's an awful lot of work (Time + Materials) for about $350 worth of Platinum. There has got to be a cheaper and easier way to recover Platinum if criminals are stealing Catalytic Converters for the precious metals they contain. In a small scale enterprise, I think ones time and money is way better spent recovering Gold and Silver. (As always, it was a Great Series of Videos)

  • @shaneyork300
    @shaneyork300 Рік тому

    A really good series!

  • @davidmccleary5540
    @davidmccleary5540 Рік тому

    Enjoyed the whole series and what I took away was gold and silver where it's at. When you are having trouble, that means nearly everyone else should not attempt platinum. Great series though

  • @Michael-db1ce
    @Michael-db1ce Рік тому

    Wow, that precipitate looked like chocolate milk. I think I was more anxious watching you do that than you were when actually doing that.

  • @jamisontaylor878
    @jamisontaylor878 Рік тому

    Excellent job it worked for me!!!!

  • @EchoJulez
    @EchoJulez Рік тому

    What a challenging refine. I knew all you needed was a steak and wine dinner with your family to figure it out.
    P.S. love the Omega timepiece.

  • @11THEFEZMAN11
    @11THEFEZMAN11 Рік тому +1

    If you don’t fail you don’t learn. I’m an artist I throw a way a lot of things that normal people would consider great.
    Now, I’m not fiddling with super dangerous chemicals but, I do get burned a lot blowing glass. I also break a lot

  • @robertsletten7466
    @robertsletten7466 Рік тому

    Nice Job ... Looks good ...

  • @brianhbinesh
    @brianhbinesh Рік тому

    Can't wait for another stock pot refining video series.

  • @frantiseklaluch6605
    @frantiseklaluch6605 Рік тому

    Hello sir, thanks, that was pretty deserved button of platinum. I am not touching platinum salts, not even with 10 feet long chlorine desinfected stick... I will buy small platinum coin (Philharmoniker) , just to have some pure platinum, but no refining... I can do cupeling PGMs into button, that is it...

  • @DisabledParkHopper
    @DisabledParkHopper Рік тому

    Never Know If ya Never Try! You did Great!!!

  • @kaylabridgetrobinson5150
    @kaylabridgetrobinson5150 Рік тому

    Loved the videos 🎉

  • @ExtractingMetals
    @ExtractingMetals Рік тому

    I enjoyed watching this series. My take away from it is that I will never try to refine PGMs because of the dangers.

  • @mrawesomeDK
    @mrawesomeDK Рік тому

    This is the longest series of nothing that ever happened I’ve ever watched 😂
    Nevertheless, your videos are always extremly fascinating and interesting 😊

  • @xKateshi
    @xKateshi Рік тому

    Great job regardless. That looked risky, be careful man, I'd rather be able to watch more of your videos.

  • @WaffleStaffel
    @WaffleStaffel Рік тому

    Aside from what's in Hoke on dental scrap & p.108, this may be of use-
    "1 part of the salt (Ammonium Hexachloroplatinate) is sufficient to impart a yellow color to 20,000 parts of water. Its insolubility in ethanol and diethyl ether permits a separation of platinum from palladium because the corresponding palladium salt is soluble." Ammonium Hexachloroplatinate(IV). Inorganic Syntheses. Inorganic Syntheses. Vol. 9. pp. 182-185

  • @ricoviselli
    @ricoviselli Рік тому

    Thanks for the filter.

  • @daviddavis4005
    @daviddavis4005 Рік тому

    Gooood evening from central Florida! Hope everyone has a great night!

  • @anthonywaite
    @anthonywaite Рік тому

    I know nothing about refining metals but what about maybe a smelting type of process for platinum almost like what Jason does for gold and silver at mbmm... is there any mix of fluxs that could oxide the iridium away maybe with a collector metal like lead or something and maybe Cupel just wanted to ask the question because I have no idea honestly no refiner i just love learning about the process buddy keep up the good work...

    • @sreetips
      @sreetips  Рік тому

      The people that I learned from didn’t teach cupel. Plus, platinum metals are so much alike that they are nearly impossible to separate with special equipment and knowledge.

  • @slimpickins09er87
    @slimpickins09er87 Рік тому

    Thanks Sreetips, you always mention the dangers of PGM's. Thankfully, you were not harmed in this series. I can honestly say this is one demonstration I have no desire to attempt. Is there any chance of a stockpot series in the near future? Is there any reason you don't separate your stock pots in gold, silver and pgm's?

    • @sreetips
      @sreetips  Рік тому +1

      Gold refining waste contains platinum so gold and platinum group go in the same stock pot. Silver is kept separate.

  • @ssofmas8473
    @ssofmas8473 Рік тому

    Hi doctor you did best job👌🏻👏👏
    Doctor for evaporation you could put off that lid that way you can rapidly vapor your solution and metal remain in your solution there is any reason you put glass on your beaker for evaporations?

    • @sreetips
      @sreetips  Рік тому

      So the toxic Pt solution did not spatter out all over the place.

  • @OnsloVest
    @OnsloVest Рік тому

    Thanks for the effort sreetips :)

  • @jamescball55
    @jamescball55 Рік тому

    Is there a report on the analysis of the metal that you had analyzed? I am a PhD chemist and I love your videos. I would do things a little differently and try to stay stochiometric as much as possible with maybe a slight excess. Your lab techniques are outstanding. And your methods work - what can I say?

    • @sreetips
      @sreetips  Рік тому

      Thank you. I’m not a trained chemist. I just do the next logical thing based on my experience.

  • @leor2830
    @leor2830 Рік тому

    Good job mate!!!!!!!!!

  • @Sanzus2
    @Sanzus2 Рік тому

    Tenacity only gets you so far! The risks are so high so I'm assuming you've got something inside driving you to do this? Got me nervous a few times with this series, good choice to wrap it!

  • @jwrappuhn71
    @jwrappuhn71 Рік тому

    Excellent.

  • @davidgreen2379
    @davidgreen2379 Рік тому

    I caught myself pouring a spoonful of sugar into my coffee while saying
    "Once these crystals go into Solution, the process will be complete"

  • @KD0CAC
    @KD0CAC Рік тому

    Forgot the ebay link ;)
    Thanks again