Indexing XRD peaks with hkl values using X'pert highscore - 25
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- Опубліковано 1 лис 2024
- In my previous video (link is given below), I have shown how to label XRD peaks with Miller Indices (hkl) values using OriginLab software. Indexing XRD peaks through OriginLab could only be done manually, while the X’pert Highscore software could do the same task automatically.
In this video, I have shown the labeling (indexing) method only. For a detailed analysis of XRD data through X’pert Highscore and OriginLab, please watch my other videos links are given below. If you have any questions, ask them in the comment section below. For more videos, please subscribe to NanoWorld. Thank you.
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Hello Sir, I am not able to do the reitvield refinefinement as you shown in your video. Always a pop window opens which says no structural data available for reitvield refinement. Please help.
Thanks, eagerly waiting for your next video. Could you please make some Detailed tutorial videos on VESTA software and also FullProf for Rietveld analysis..?
Very nice... eagerly waiting for your next video...
Hi, thank you for your so much useful videos. I followed the steps as you said, but I get this error in the rietveld step: No structural data for simulstion/ negative intensities in scan data point. Can you please help me. Thank you.
How to show William-Hull in X'Pert HighScore sir?
@NanoWorld I try to Label XRD Peaks with Miller Indices (hkl). But there is not any option in of rietvield in Analysis. Can you help me what is the problem ?
same issue, the analysis tab contains only two features, cluster analysis (hidden) & search and match
is ur issue solve? i got same issue
@@sharminewz5632 NO still same issue
Please upload a video about how to install x pert high score software.
Excellent video. Thanks a lot!!!
Glad you liked it!
You are great. Thank you very much.
sir. thanks for this video. but I am not able to do reitveld refinement. once I do start refinement it shows No data for refinement. How to solve this. please do help
Why did you strip Ka-(alpha2) frequencies in this video? you didnt strip them in your previous video
Hi Sir, I am facing a problem in Rietveld refinement..Errors are coming at the time of Rietveld analysis..Could you please tell me how to do Rietveld analysis?
I have the same problem .
Please if you solve it tell me how?
Thanks for the video, xpert highscore is not working in my case? any solution?
Hi, Thanks for the great video, but I have some queries regarding the hkl values. I have the same hkl values for zinc oxide as in this video, but they do not match the literature data. For example, in literature, the first three planes are namely (100),(002), and (101). But in the Xpert report, we can find that it is (010),(002), and (011). Can you explain these discrepancies?
Hello sir....how can I add more JCPDS data in XPERT High Score PLUS
Hi! Thanks for the great video. Performing the K-alpha 2 stripping generates a negative peak in my diffractogram, which prevents Rietveld refinement. Please advise!
Hlw sir
I need your help
kindly provide the link of your current version of xpert highscore software 3.5
rietveld refinement is not working in my xpert high score plus, so I can't find (h k l) values. please solve the issue.
Hi sir..I have followed same steps that you have told for background removal but instead of removal, background became more prominent... please guide what's the mistake in it?
HI sir i am new to origin and xpert highscore . pls tell the procedure how you create the file ZN1(XRD).ASC
FOR ME IT IS SAVING FILE AS OPJU
Hi, Thanks for this video with indexing the Miller indices. I have a question. If miller indices on experimental spectra are different from reference data (on the pattern list), what does this mean? something wrong?
Then either you are matching it with the wrong JCPDS card, or your sample is not successfully synthesized.
Sir after selecting metal from periodic table when I proceed next it's show no result found i have some issue with my high score
Hi sir, How can I calculate the value of young's modulus and Poisson's ratio from XRD data?
How to save four data files in one .ASC file? or to export all the data files after plotting in Highscore and then export it in origin?
Sir only ASc file will open in it can we open any other file in it please reply sir
Please can u provide me your mail please sir
Sir while refinement...my report shows problem.can you tell me what it is and it is due to what.
Problem is
No structural data for simulation
Negative intensities in scan data point.
Please give me solution
I have the same problem .
Please if you solve it tell me how?
which file format of origin open in Xpert highScore plus??
great help
thanks a lot
Thank you very much, very helpful video, but, why when I click start Rietveld refinement, then I keep getting no valid atom positions available?
Here is the solution
ua-cam.com/video/ppLoZvjgad0/v-deo.html
@@nanoworld6122 Thank you very much. You are very helpful.
Please any one reply which file of xrd u open in it sir
Hi sir in my analysis, match result is showing that no Candidate found . What do to in such cases.
sir how to calculate lattice parameter of composite film Polyvinyl Achohol (PVA)-LaFeO3 with different concentrations
pls drop the link to this version of xpert highscore
can you share me the data base which supports xpert highscore 3v
Thanks a lot, could u make.a video for how to calculate the ratio between the pahses in one material? for example I have Monoclinic... and tetragonal Phase in my.material and I.need to calculate the ratio between them either by XRD or retieveled refienment, Thanks a lot
Noted! I will upload soon.
In my software execute option is not opening what to do sir please
Hello, sir when i go to rietveled - start to rietveled then it shows No structural data for simulation/refinement. What can i do sir?
Sir, Can you share your X'pert Highscore software link to download
I'm facing an problem report stating negative intensity in scan data points so how to resolve this and add peeks of hkl value can anyone please help me out
Sir, when I give rietveld, it is showing as no valid atom positions available. What to do Sir
Did you get the answer ?
Can we find hkl values in excel ?
No
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