Rietveld refinement in 4 minute │The simplest way to refine XRD results │ using MAUD
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- Опубліковано 15 вер 2024
- This a video tutorial on Rietveld refinement easily and quickly. #RietveldRefinement is generally very lengthy and complex job. If you need to do Rietveld refinement a few times, why should you learn it by spending several days? Don't worry, there is one way by which you can do Rietveld refinement in just 4 minutes.
This is possible using #MAUD software.
For details: inscilab.com/t...
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Thank you for a short and clear video. You haven't changed the instrument parameters in this video, I thought you need to use and calibrate the correct instrument type in maud
I hope this video will help the people who wanna perform Rietveld refinement. Just a quick suggestion, Its better to speak while writing so that this can be more helpful to the audience
Awesome. Very useful.
I request you to explain, rather than music. What type of file is required to be opened in MAUD ? Is it free software?
YES it is free!
maud.radiographema.eu
File: .dat or .xrdml
Thank you very much for your comment.
If I don't have CIF file for my compound, then how do I get X, Y, Z, B and Occ values? Please help me in finding them.
If you found out how, tell me. Please)
Nice work! I really loved it! When can we get the next video? I really want to know how we can reduce the sigma value even more.
hi...I wanted to calculate the weight percentage of different compounds in a composite .To be specific quantity of formation of mullite as it may contain alumina or silica also....how can I do that using rietveld refinement...can you please let me know the procedure?
You are a savior, right now for me! Would these calculations be accurate enough to report in international journals?
For structure confirmation (to report the crystal structure and space group, indexing peaks) this will be okay, I guess.
But, if in your paper, structure is one of the important topics, then I suggest you to do FullProf refinement. Because, 1) MAUD is not recognized well 2) the method I showed takes care only very preliminary things.
There are 3 videos on FullProf in my channel itself. I am sure those will not be very hard.
If you want to do MAUD as an expert you can contact inventor Luca Lutterotti. He is very humble to help. let me know if you want his contact.
@@InSciLab Hey thanks for the help. Although I have downloaded the Fullproof, I would still like his contact. Can you mail that to me at hwadikar@asu.edu, please?
Hi! I am using
monpaphomic.wixsite.com/dersoriru/single-post/2018/02/20/Foolproof-Xrd-Software-Free-16
to get Fullproof but for some reason it did not work and my Chrome crashed. Also an extension 'Pulse got added'.
Is there anyother link? Please help!
@@harshwardhanwadikar793 thanks for your wonderful comments to the other video also.
I have sent email with contact details of Dr Luca Lutterotti.
the official link: www.ill.eu/sites/fullprof/
So how do you reduce the sig value further...also, I have a good sig already, but my Rwp is still bigger than 10, how can I reduce it?
Sir, your videos are very helpful and knowledge full. If I do not get cif files of some molecules then how can I do refinement of this.
I have composit materials XRD , then how can I refine it using full prof.
Please help me.
I have the same problem now. If you can overcome it, can you help me?
Is there any reason you're not supposed to maximize the window? I installed MAUD and opened it, but the window is much smaller and doesn't show the graph like your video shows.
I appreciate your work thanks...Do you think it is possible for high entropy alloys thin film, containing at least 5 elements (CoCrMoMnNi) ....As i input all these elements in Craystallography dtata base but nothing shown....
Please make video how to convert x axis value into -x axis in origin. For the comparison of simulated data and experimental data
I guess you should go to "Windows - Script Window" and type "layer.x.reverse=1", then press Enter. You should know layer name for doing this as it may be "layer2" or "layer3".
Thank you for this helpful video. I have a problem regarding the theta angles, do you know how to solve it?
Basically the theta values of my peaks and theta values found in phase cif. files are not exactly the same, so I can't apply the Rietveld refinement properly.
Find a better CIF. Maybe same structure but different composition is okay
Its really nice video, but in my case Maud taking to much time for download
Try downloading from other computer.
Thank you But How can interpretation clay mineral XRD chart with three treatment (Glycol and Heating)?
Could not understand the question? Maybe I didn't understand as I don't know this field
I am not able to save or copy image done after rietveld...please help..i want to save images. How to do this ?
I need help in MAUD for finding XRD FWHM peaks
sir how to calculate lattice parameter of composite film Polyvinyl Achohol (PVA)-LaFeO3 with different concentrations
Do you see any paper on Polyvinyl Achohol (PVA)-LaFeO3? What do they say....
In general, I would ask you to check other refinement tutorials.
I am very interessting by this program. I want to learn more. Who can help me please ?
Can i get FWHM values for the XRD peaks in maud?
what is the difference beteewn MAUD and FPS?
what is the difference in MAUD and FPS?
I do not have xrdml fail, but I have simple CSV file which seems can be loaded well, but strangely, it shows energy ev instead of 2-Thetha for x-axis, and failed to refine the data... any hint?
What is your original file format (before CVS)? Use that file to convert to xrdml. Read about file conversion here inscilab.com/tips-tricks-tutorials/xrd-data-file-conversion-any-format-to-17-standard-format/
hOW DO YOU CONVERT FROM MAUD TO ORIGIN
Hello. I would like to know how I can use Maud to calculate an amorphous percentage
For that you don't need Maud. You can do it using Origin itself. Let me know if you want a tutorial video showing how to do that using origin.
@@InSciLab I just found a tutorial for that using Origin. Thanks for your collaboration 😀
@@InSciLab dear prof, can you give a tutorial video for precentage calculation using origin? Thx
tks u, btw could u make a tutorial by using Origin program?
Using Origin? Do you mean refinement using Origin?
yeah, it's so kindly if u make some video tutorial introduce some functions of Origin Pro and how to use it?
Thank sir so much!
Dear Sir, how can I get next this video? Thank you!
Do you mean video on refinement? There are videos on Fullprof but this is the only one on MAUD.
@@InSciLab You said next video you will show how to reduce "sig" value so I expected to that.
@@dungnguyenquoc116 Okay. I understood. For better Sig value use FullProf. There are 2 tutorials after this video. In one video I use the value got from MAUD and use them in Fullprof for further refinement.
@@InSciLab Thank you sir, I will try ^^
Anyone can help me how to the save file in the end of Maud software?
Is it possible to connect MAUD with COD?
I can't use this like your video because compute function doesnt work in my work. Could you let me know how to solve this error?
I didn't understand the problem. Can you please elaborate the issue?
following pushing compute button, it does not be showed like yours
I guess you have added CIF or Data file in wrong place. Check the video carefully and follow.
CIF or Data can be added to any place but finally will not show any result. I am not sure about the issue you are facing.
MY SAMPLE IS Ba.9-xSr.1GdxTiO3 plz help me to calculatelattice parameter. from my data i showed my structure phase change to tetragonal phase to cubic phase so now in which formula can i apply? and here (cod) i did not get my sample and space group
What is range of value of x?
If it is x
How does it work with organic compounds ?
It depends on the structure and experimental data. you can try with organic and let me know how does it work. I have no experience with xrd of organic sample.
please help me .... i have powder xrd peaks
how to find the spacegroup lattice parameter and atomic position ???
did you check our website?
@@InSciLab please give me the link
@@G.Thamizharasan There are a few articles which may help you.
inscilab.com/category/tips-tricks-tutorials/xrd/
Which should be preferred Maud or fullprof?
Fullprof. If you don't have much time to learn or refinement result is just a supporting data, have not much importance then you may use Maud. This is my personal opinion. Otherwise both are okay depending on usage and knowledge you have.
@@InSciLab okay thank you.. Can I obtain lattice parameters using Maud?
Yes.
How to do for Cobalt ferrite like CoFe2O4. I tried but no use. Plz help to do.
Did you watch the other video? There I explained how to start. Please follow the steps. ua-cam.com/video/FlrP3rRgyWI/v-deo.html
Follow it and let me know if you have any doubt. Your space group will be F d -3 m :2. CIF file is also available in the COD database.
Sir rirgt panel means what? I did not understand
Sorry. It's a typo. It's not rirgt. It's right.
Hi! How can i have the xrd file, i do not have one? Thnx
Check it here: inscilab.com/tips-tricks-tutorials/easiest-best-way-to-do-rietveld-refinement-using-fullprof-software-suit-2/
how to get cif file if my composition is not reported
You can find out most similar structure. for example if you don't get CIF for PbTiO3 then you can search for CaTiO3 or BaTiO3 as these are having similar structure.
I am a student in a master 's degree.I am rietveld with maud but it is hard because amorphous peak.And the crystallite size of amorphous peak is very small as 2 ~ 3nm.could you help me ..?
Sure. I will try to help you. Can you tell me about your material. Composition, possible structure and any other useful information.
Thank U !.. Can you tell me your e-mail address?...
The indium metal was dissolved in nitric acid, diluted in water, and adjusted to pH 7 with ammonia water to form In (OH) 3. However, I have two peaks of In (OH) 3 and InOOH, and I want to see the phase ratio, the atom position, and the lattice parameter.
InOOH is an amorphous phase, and when I search on PDXL, it says InOOH, but I do not know if it is honest.
I don't have experience with such system. But, I can try. email me at contact@easywayhowto.com
Thank U ㅜㅜ
Can you sent me the file: BA2_C700_SLOW.xrdml. Thank you.
Sadly for download only very old files are available!
Did you check the page (link is given in the other comment)?
Just few months ago, the official site of MAUD was working. Now it is not working. The latest software can only be downloaded from their official site.
Yes, maud.radiographema.com is not working. I downloaded software from www.ccp14.ac.uk/ccp/web-mirrors/lutterotti/~luttero/maud/maudWebStart/maudWebStart.html The Maud Web start is 2004 version and Maud installer for Windows is of 2003, so its not like in video.
If you can drop the never version I would be very thankful.
how can I obtain the crystallite size?
Go to the result file. The calculated values for crystallite size for
each peak are listed with the peak list. read carefully as the columns
are spaced very closely.
hm..i did it as you showed us in the video. but i only could find the d-spacing values for each peak. (e.g for (001) --> 4.0863295).
Refinment of respective options from refine wizard is necessary to get crystallite size.
Try if you don't find let me know.
where is next video of this series sir
Hi Sanjay, Thanks for asking. It will come soon. I have started the detailed tutorial.
I am using MAUD and Full Prof past two years Sir by seeing videos and books so some doubts are there can you please help me Sir.
Is that possible to get ascii of MAUD data of all because only one file I am getting computed one as ascii difference file I do not know how to get as whole like in Full Prof
I am confused.
I guess, I don't know what you are looking for.
If this can help you: Copy the entire result and paste it to a new text or word file.
I have a .raw file
Try it. if doesn't work, convert it to .dat or .xrdml using PowDLL
Nothing for 32bit 😢
MAUD runs on both 32 and 64.
I have notice maud\lib\com.github.tschoonj.xraylib.jar the file is corrupt. Why?
@@helnikurniawatizebua7325 I have no idea on that.
Can you tell me where we can see the lattice parameter of sample?
@@helnikurniawatizebua7325, do you mean, you want to find out lattice parameters in MUD?