AIF NC State University
AIF NC State University
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Basic Vacuum Technology & Vacuum Pumps
Watch this video to learn about the fundamentals of vacuum technology, good vacuum practices, trouble shooting, and more.
The AIF would like to thank Fred Stevie for this presentation. Fred has 40 years of experience with vacuum instrumentation and is an American Vacuum Society instructor.
Переглядів: 151

Відео

2024 Nanopatterning with a Focused Ion Beam (FIB)
Переглядів 2145 місяців тому
A focused ion beam (FIB) can nanopattern samples by selectively depositing or sputtering materials. In this video, Nichole Cates of Smart Material Solutions, Inc. discusses FIB patterning processes and demonstrates FIB nanopatterning on the Quanta 3D DualBeam FIB/SEM in the AIF at NCSU.
Powder Sample Preparation
Переглядів 1637 місяців тому
This video shows how to prepare powder samples for individuals that use high vacuum analytical equipment (like an SEM or FIB). As loose powders can cause serious issues to these microscopes, it's important to safely prepare these types of samples to prevent damage. If you have any questions or would like to know more, please email Roberto Garcia at rgarcia@ncsu.edu.
Allied High Tech Multiprep Alignment
Переглядів 27310 місяців тому
Watch this short video to learn how to align the multiprep instrument prior to use.
Sputter Coating: How to Use the Cressington Sputter Coater at the AIF
Переглядів 219Рік тому
This video will show you how to the use the Cressington Sputter Coater to coat samples with a fine gold palladium film.
Quanta FIB Lift Out
Переглядів 447Рік тому
00:00:00 Introduction 00:00:58 Instrtument Interface 00:01:42 Wake Up Ion Beam 00:02:28 Set Eucentric 00:09:17 Pt Ebeam Deposition 00:16:49 Ion Beam Pt Deposition 00:21:05 Hog-Out 00:26:43 Clean-Up cut 00:33:20 J-Cut 00:42:59 Needle Attach 00:55:07 Grid Clean and Notch 01:02:35 Grid Attach 01:05:08 Needle Cut Away 01:10:31 Initial Thinning 01:22:04 Final Thinning 01:41:19 Final Polish
Goodbye Verios, Hello SU8700 SEM
Переглядів 390Рік тому
See the decommission of AIF's Verios and the installation of our new SU8700 SEM. The Verios was acquired in 2014 and has helped thousands of users with their research. Special thanks to Roberto Garcia for this recording.
FIB Si TEM Prep
Переглядів 686Рік тому
00:00:00 Intro 00:01:40 Eucentric 00:07:58 Electron Beam Pt Deposition 00:17:11 Ion Beam Pt Deposition 00:24:35 Hog-Out 00:29:33 Clean-up Cut 00:36:07 J-Cut 00:41:07 Needle Attach 00:43:07 Clean Omniprobe Needle 00:45:26 Touch Needle to Sample 00:46:35 Needle Attach 00:50:45 Grid Attachment 01:01:57 Final Thinning 01:34:47 Final Polish
Nanopatterning with a Focused Ion Beam (FIB)
Переглядів 1,6 тис.Рік тому
A focused ion beam (FIB) can nanopattern samples by selectively depositing or sputtering materials. In this video, Nichole Cates of Smart Material Solutions, Inc. discusses FIB patterning processes and demonstrates FIB nanopatterning on the Quanta 3D DualBeam FIB/SEM in the AIF at NCSU.
FIB Tips for TEM Sample Preparation
Переглядів 840Рік тому
This FIB video shows intermediate users some shortcuts and tips to improve the TEM sample preparation process.
How to Repair a Dry Scroll Pump
Переглядів 6 тис.Рік тому
This video demonstrates how to repair a dry scroll vacuum pump. It shows how to remove a worn seal and replace it with a new one to make the pump function like new! If you have questions, please email our Operations Manager, Roberto Garcia, at rgarcia@ncsu.edu.
Basic Focused Ion Beam Demo
Переглядів 2,3 тис.2 роки тому
Rudimentary introduction for Focused Ion Beam (FIB) - lecture and demonstrations
FIB Patterning Demonstration - AIF + Smart Material Solutions
Переглядів 9912 роки тому
DualBeam FIB/SEMs like the Quanta 3D FIB/SEM and the Helios 5 Hydra plasma FIB/SEM at the AIF can nanopattern both by removing material with FIB milling processes and growth of material with FIB deposition. In this video, Nichole Cates with Smart Material Solutions shared her experience FIB patterning features ranging in size from a few hundred nanometers to tens of microns on these systems. Th...
Vacuum Technology - Gauges
Переглядів 2,3 тис.2 роки тому
In this video, Fred Stevie gives an introduction on pressure measurement gauges. Interested in learning more? Email aif-contact@ncsu.edu for more information.
Vacuum Technology - Vacuum Pumps
Переглядів 2,9 тис.2 роки тому
In this video, AIF's Surface Science Lab Manager, Fred Stevie, gives an introduction on vacuum pumps. Interested in learning more? Email aif-contact for more information.
Introduction to Vacuum Technology
Переглядів 6 тис.2 роки тому
Introduction to Vacuum Technology
EDAX Apex EDS Introduction
Переглядів 1,2 тис.2 роки тому
EDAX Apex EDS Introduction
2021 Carolina Science Symposium
Переглядів 1762 роки тому
2021 Carolina Science Symposium
AIF Mendix Instructions
Переглядів 3923 роки тому
AIF Mendix Instructions
AIF's Rigaku Bragg-Brentano
Переглядів 7663 роки тому
AIF's Rigaku Bragg-Brentano
Phase Identification with HighScore Plus
Переглядів 36 тис.3 роки тому
Phase Identification with HighScore Plus
General Introduction to X-ray Computed Tomography
Переглядів 6 тис.3 роки тому
General Introduction to X-ray Computed Tomography
X-ray Tomography of a Bee
Переглядів 2493 роки тому
X-ray Tomography of a Bee
Additive Manufacturing Copper Alloy
Переглядів 2523 роки тому
Additive Manufacturing Copper Alloy
XRM at AIF - Bones
Переглядів 793 роки тому
XRM at AIF - Bones
Dr. Jacob Jones - 2020 R. J. Reynolds Tobacco Company Award Distinguished Lecture
Переглядів 3403 роки тому
Dr. Jacob Jones - 2020 R. J. Reynolds Tobacco Company Award Distinguished Lecture
Silicon FIB Lift Out
Переглядів 7513 роки тому
Silicon FIB Lift Out
Practical SEM: Electron Optics
Переглядів 3,7 тис.3 роки тому
Practical SEM: Electron Optics
2020 AIF Virtual Open House & User Appreciation
Переглядів 2484 роки тому
2020 AIF Virtual Open House & User Appreciation
Gas Cylinder and Vacuum Safety
Переглядів 5844 роки тому
Gas Cylinder and Vacuum Safety

КОМЕНТАРІ

  • @EliseoBurcheri
    @EliseoBurcheri 2 місяці тому

    nice

  • @mani2263
    @mani2263 4 місяці тому

    Very well explained presentation!

  • @poompato
    @poompato 4 місяці тому

    SU8700 SEM of hitachi compare Verios thermo for the nano material whis is best image and performace I want buy use in my lab

  • @joshuasantos9002
    @joshuasantos9002 4 місяці тому

    How did you create the bitmap file and how did you ensure that the resolution would be good enough for the microscope?

  • @tamilcouples0626
    @tamilcouples0626 4 місяці тому

    Very very useful... Thank you for sharing this video❤❤🤝🙏💐💐

  • @ioannams2709
    @ioannams2709 5 місяців тому

    Hi, what is this green material you use on your sample holder?

    • @aifncstateuniversity4762
      @aifncstateuniversity4762 4 місяці тому

      Hello and thanks for your question! The lab manager that created this video is no longer with the AIF but the current lab manager uses Orthodontic wax strips manufactured by Kulzer LLC.

    • @ioannams2709
      @ioannams2709 4 місяці тому

      @@aifncstateuniversity4762 Thank you!!

  • @noreezy4991
    @noreezy4991 6 місяців тому

    heat gun at a temperature below the operating temperature of the components is almost guaranteed to make that process of cleaning easier.

  • @gabbicolano
    @gabbicolano 7 місяців тому

    Amazing introduction!

  • @LondonA2Z
    @LondonA2Z 7 місяців тому

    Very beneficial. Thank you.

  • @bulutgezer4105
    @bulutgezer4105 8 місяців тому

    Thanks for your detailed information; Definitely a very useful video. but the cameraman has no idea what he is doing.

  • @DanielFuller-c8x
    @DanielFuller-c8x 8 місяців тому

    Any tips and tricks for a Varian 300 scroll pump?

  • @philip2.2.12
    @philip2.2.12 8 місяців тому

    9:08 certain vacuum chambers use cooling water that is above room temperature specifically to keep any water from condensing on the inside

  • @gauravkumarph.dstudent2418
    @gauravkumarph.dstudent2418 8 місяців тому

    that was very useful to understand.

  • @saysoonkim9561
    @saysoonkim9561 10 місяців тому

    Thank you!

  • @NashatAbdel-Gawad
    @NashatAbdel-Gawad 11 місяців тому

    how can i insert crystallite size values in the report

  • @mendozaolguinjuliana8431
    @mendozaolguinjuliana8431 Рік тому

    Thanks for the video!

  • @AsifKhan-kc2rg
    @AsifKhan-kc2rg Рік тому

    Greetings sir I have find extra peaks in my xrd data can you please help me how can I find the phase for these extra peaks. Also please tell me which software u are using Thanks regards

  • @housevenn6912
    @housevenn6912 Рік тому

    Goodbye Verios. I really want to take a photo with her.

  • @ZLQIAN
    @ZLQIAN Рік тому

    nice introduction to FIB !

  • @kitousaya4336
    @kitousaya4336 Рік тому

    Thank you so much

  • @poly_hexamethyl
    @poly_hexamethyl Рік тому

    4:56 This chart shows that nature doesn't really abhor a vacuum. It's actually what most of the universe is.

  • @housevenn6912
    @housevenn6912 Рік тому

    curious how this cross pattern is made?

    • @RobertoGarcia-tc5xq
      @RobertoGarcia-tc5xq Рік тому

      If you are talking about the cross pattern that appears about 4:13 into video, it is the standard alignment and calibration sample that comes with the instrument.

    • @housevenn6912
      @housevenn6912 Рік тому

      @@RobertoGarcia-tc5xq Yes. That's what I want to ask. Thanks for your answer!

  • @tem4eva
    @tem4eva Рік тому

    Lots of good tricks and tips here. Thank you!

  • @aleshinteregger8554
    @aleshinteregger8554 Рік тому

    thank you

  • @JerryChangTaiwan
    @JerryChangTaiwan Рік тому

    Thank you for the fantastic video!

  • @mevynofficial1683
    @mevynofficial1683 Рік тому

    Awesome video and very helpful and easy to understand. Thank you!

  • @Erhannis
    @Erhannis 2 роки тому

    Thanks for the knowledge! Was the Signals and Detectors lecture ever uploaded? I don't see it in AIF's videos list.

  • @jweber2954
    @jweber2954 2 роки тому

    Thanks for publishing this

  • @eng.tadesseendaleteferra3706
    @eng.tadesseendaleteferra3706 2 роки тому

    please link to download

  • @cosanostra8341
    @cosanostra8341 2 роки тому

    Hello, thank you very much for the explanation!! I did nanoidentation on a photoresist with 3 different layer thicknesses (4.5um, 5.2um and 6.5um) with a penetration depth of 500nn. i'v come to the conclusion that when the thickness of the photo resist is bigger, then the foto resist is harder. Do you have an idea why?? Thank you very much!!!

    • @aifncstateuniversity4762
      @aifncstateuniversity4762 Рік тому

      In general, film thickness and film hardness is known to typically be negatively correlated for thin films (meaning, increasing thickness =increasing hardness). However, these appear to be thicker films with a very shallow indentation depth by comparison - so the photoresist could essentially be considered a bulk material at this scale and thin film behavior may not be applicable in this case. It's possible this explains your result, but would encourage you to consider there may be other factors contributing to the higher measured hardness for the top most surface of this otherwise thicker film.

  • @phuongnguyen-nb5sd
    @phuongnguyen-nb5sd 2 роки тому

    link dowload plz

  • @vvrao7006
    @vvrao7006 2 роки тому

    Very nice

  • @sreejithpisharady1044
    @sreejithpisharady1044 2 роки тому

    This video is very helpful . Will you please send me JCPDS card number 41-1478

  • @anindita6913
    @anindita6913 2 роки тому

    Great

  • @housevenn6912
    @housevenn6912 2 роки тому

    Great video. Looking forward to the data analysis part. Thanks for sharing. Go wolfpack.

  • @DidarulIslam
    @DidarulIslam 2 роки тому

    Shout out to Fred! Very well made content. Thank you AIF!

  • @kriangsakriewklang24
    @kriangsakriewklang24 2 роки тому

    Thank you very much , such a informative video!

  • @Max-cu8zu
    @Max-cu8zu 2 роки тому

    Great video!

  • @prakashgandhal498
    @prakashgandhal498 2 роки тому

    I want to buy x-ray computed tomography liquid pls guide me it's urgent

  • @prakashgandhal498
    @prakashgandhal498 2 роки тому

    Sir i want to buy x-ray computed tomography liquid wher it's available pls guide me it's urgent

  • @muhajirsam5070
    @muhajirsam5070 2 роки тому

    how to display pattern label cubic (blue), Circle (green)

    • @aifncstateuniversity4762
      @aifncstateuniversity4762 2 роки тому

      Hi there, If you want to see symbols at the top of each selected phase: To select this option, go to Document settings. In the bottom right corner, you will see "Show Pattern Markers" - select it, and apply.

    • @alymohamed1014
      @alymohamed1014 Рік тому

      @@aifncstateuniversity4762 would you please show it with pictures? because I could not find it

    • @arragsda
      @arragsda Рік тому

      @@alymohamed1014 UA-cam doesn't allow pictures to be posted in the comments. If you'll send us your email address, we can send you the picture.

  • @MuhammadAliSharBaloch
    @MuhammadAliSharBaloch 2 роки тому

    Nice 👍

  • @djricky89999
    @djricky89999 2 роки тому

    Wow fantastic equipment

  • @eskilandreasson8204
    @eskilandreasson8204 2 роки тому

    Great video/course!! Thanks for sharing 😀🙏

  • @4sambath4sambath75
    @4sambath4sambath75 2 роки тому

    Thanks for the seminar. Was great.

  • @戴铭基-f9h
    @戴铭基-f9h 3 роки тому

    amazing

    • @prakashgandhal498
      @prakashgandhal498 2 роки тому

      Pls help me i want xray computed tomography liquid if any idea where it's sell pls message me urgent

  • @thomassmart9077
    @thomassmart9077 3 роки тому

    Great seminar, Chris.

  • @jamesjoseph884
    @jamesjoseph884 3 роки тому

    What type of secondary ions does collision with Uranium brings in?

    • @aifncstateuniversity4762
      @aifncstateuniversity4762 2 роки тому

      It is most likely a positively charged U ion formed. In some cases, negative ion of U could also form depending on the chemical matrixes.

  • @dongdongzhu6700
    @dongdongzhu6700 3 роки тому

    very very nice talk, could you explain why we should keep our samples dry when we run SIMS analysis (Si isotopes)? Is it ok if we have solids with .h2O within our solid particle (for example CuSO4.H2O)?

    • @aifncstateuniversity4762
      @aifncstateuniversity4762 3 роки тому

      Since the pressure of the analysis chamber in ToF is in the range of 10E-9 mbar, without a cryo stage, only solid samples can be analyzed. Liquid or materials containing water will dehydrate under the high vacuum and it is also detrimental to the pump.

  • @Zahraa-uu2wb
    @Zahraa-uu2wb 3 роки тому

    Many thanks doctor🙏🌹